Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering

Calcium phosphate (CaP) compounds like hydroxyapatite and tricalcium phosphates are considered to be very important biomaterials. This study used RF-magnetron sputtering (RF-MS) to deposit CaP onto 316L SS. Due to the complex nature of the effect of different sputtering parameters on the quality and...

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Main Authors:	Toque, Jay Arre, M., Hamdi, A., Ide-Ektessabi, Iis, Sopyan
Format:	Article
Language:	English
Published:	World Scientific Publishing Company 2009
Subjects:	TS Manufactures
Online Access:	http://irep.iium.edu.my/11423/ http://irep.iium.edu.my/11423/ http://irep.iium.edu.my/11423/ http://irep.iium.edu.my/11423/4/Effect_of_the_processing_parameters_irep_ID11423.pdf

id	iium-11423
recordtype	eprints
spelling	iium-114232012-05-12T14:26:38Z http://irep.iium.edu.my/11423/ Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering Toque, Jay Arre M., Hamdi A., Ide-Ektessabi Iis, Sopyan TS Manufactures Calcium phosphate (CaP) compounds like hydroxyapatite and tricalcium phosphates are considered to be very important biomaterials. This study used RF-magnetron sputtering (RF-MS) to deposit CaP onto 316L SS. Due to the complex nature of the effect of different sputtering parameters on the quality and integrity of the coatings, there is a need to further investigate those parameters collectively. An L9(34) orthogonal array was employed to design the experiment that was used to investigate four important coating parameters which include RF-power, argon gas flow rate, deposition time and post-heat treatment conditions. The coating composition and structure were evaluated using XRD, EDX and FTIR. The mechanical property was measured in terms of the adhesion strength using a microscratch testing machine. The response graph of the results revealed that the interfacial strength of CaP was mainly influenced by the deposition power, while the coating thickness was predominantly affected by the argon gas flow rate. High adhesion strength was achieved when the coatings have at least 2 μm thickness and deposited at a working pressure of 12 m Torr. ANOVA on the control factors helped rank the parameters accordingly in order of importance. Based on the response of the control factors, it was found that optimum adhesion strength could be achieved by depositing the coatings using the following parameters: 10 sccm of argon gas flow rate; 150 W of RF power; and 16 h of deposition World Scientific Publishing Company 2009 Article PeerReviewed application/pdf en http://irep.iium.edu.my/11423/4/Effect_of_the_processing_parameters_irep_ID11423.pdf Toque, Jay Arre and M., Hamdi and A., Ide-Ektessabi and Iis, Sopyan (2009) Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering. International Journal of Modern Physics B, 23 (31). pp. 5811-5818. ISSN 0217-9792 ; 1793-6578 http://www.worldscinet.com/ijmpb/ijmpb.shtml 10.1142/S021797920905479X
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English
topic	TS Manufactures
spellingShingle	TS Manufactures Toque, Jay Arre M., Hamdi A., Ide-Ektessabi Iis, Sopyan Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering
description	Calcium phosphate (CaP) compounds like hydroxyapatite and tricalcium phosphates are considered to be very important biomaterials. This study used RF-magnetron sputtering (RF-MS) to deposit CaP onto 316L SS. Due to the complex nature of the effect of different sputtering parameters on the quality and integrity of the coatings, there is a need to further investigate those parameters collectively. An L9(34) orthogonal array was employed to design the experiment that was used to investigate four important coating parameters which include RF-power, argon gas flow rate, deposition time and post-heat treatment conditions. The coating composition and structure were evaluated using XRD, EDX and FTIR. The mechanical property was measured in terms of the adhesion strength using a microscratch testing machine. The response graph of the results revealed that the interfacial strength of CaP was mainly influenced by the deposition power, while the coating thickness was predominantly affected by the argon gas flow rate. High adhesion strength was achieved when the coatings have at least 2 μm thickness and deposited at a working pressure of 12 m Torr. ANOVA on the control factors helped rank the parameters accordingly in order of importance. Based on the response of the control factors, it was found that optimum adhesion strength could be achieved by depositing the coatings using the following parameters: 10 sccm of argon gas flow rate; 150 W of RF power; and 16 h of deposition
format	Article
author	Toque, Jay Arre M., Hamdi A., Ide-Ektessabi Iis, Sopyan
author_facet	Toque, Jay Arre M., Hamdi A., Ide-Ektessabi Iis, Sopyan
author_sort	Toque, Jay Arre
title	Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering
title_short	Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering
title_full	Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering
title_fullStr	Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering
title_full_unstemmed	Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering
title_sort	effect of the processing parameters on the integrity of calcium phosphate coatings produced by rf-magnetron sputtering
publisher	World Scientific Publishing Company
publishDate	2009
url	http://irep.iium.edu.my/11423/ http://irep.iium.edu.my/11423/ http://irep.iium.edu.my/11423/ http://irep.iium.edu.my/11423/4/Effect_of_the_processing_parameters_irep_ID11423.pdf
first_indexed	2023-09-18T20:20:45Z
last_indexed	2023-09-18T20:20:45Z
_version_	1777408089895469056

Effect of the processing parameters on the integrity of calcium phosphate coatings produced by RF-magnetron sputtering

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