Mechanochemical synthesis of sodium doped hydroxyapatite powder

Bioactive hydroxyapatite (HA) with nanosized spherical shape has been synthesized through mechanochemical synthesis of calcium hydroxide and diammonium hydrogen phosphate. Sodium ion has been doped into HA by using sodium hydroxide precursor in a dry mixture of Ca(OH)2 and (NH3)2HPO4. Both Na-free H...

Full description

Bibliographic Details
Main Authors:	Syed Abu Bakar, Sharifah Adzila, Sopyan, Iis, Singh, Ramesh, Pusparini, Erlani
Format:	Article
Language:	English
Published:	Scientific Publishers of India 2013
Subjects:	TA401 Materials of engineering and construction
Online Access:	http://irep.iium.edu.my/31712/ http://irep.iium.edu.my/31712/ http://irep.iium.edu.my/31712/1/IJCA_52A%286%29_739-743.pdf

id	iium-31712
recordtype	eprints
spelling	iium-317122013-08-30T02:27:55Z http://irep.iium.edu.my/31712/ Mechanochemical synthesis of sodium doped hydroxyapatite powder Syed Abu Bakar, Sharifah Adzila Sopyan, Iis Singh, Ramesh Pusparini, Erlani TA401 Materials of engineering and construction Bioactive hydroxyapatite (HA) with nanosized spherical shape has been synthesized through mechanochemical synthesis of calcium hydroxide and diammonium hydrogen phosphate. Sodium ion has been doped into HA by using sodium hydroxide precursor in a dry mixture of Ca(OH)2 and (NH3)2HPO4. Both Na-free HA and Na-doped HA (1% - 9%) are characterized by X-ray diffraction and Fourier transform infrared analyses. Reduction of the peak intensity and adsorption bands is observed with increasing Na+ concentration in the Na-doped HA structure. Increasing Na+ content expands the lattice parameters and unit cell volume of HA, while the crystallite size and degree of crystallinity decrease with increasing Na+ level. A mixture of rods and spheres are found in the Na+ doped HA. Characterization of the obtained powder suggests that Na doped HA has a potential to be used in clinical applications. Scientific Publishers of India 2013-06 Article PeerReviewed application/pdf en http://irep.iium.edu.my/31712/1/IJCA_52A%286%29_739-743.pdf Syed Abu Bakar, Sharifah Adzila and Sopyan, Iis and Singh, Ramesh and Pusparini, Erlani (2013) Mechanochemical synthesis of sodium doped hydroxyapatite powder. Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 52A. pp. 739-743. ISSN 0975-0975 (O), 0376-4710 (P) http://nopr.niscair.res.in/handle/123456789/18707
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English
topic	TA401 Materials of engineering and construction
spellingShingle	TA401 Materials of engineering and construction Syed Abu Bakar, Sharifah Adzila Sopyan, Iis Singh, Ramesh Pusparini, Erlani Mechanochemical synthesis of sodium doped hydroxyapatite powder
description	Bioactive hydroxyapatite (HA) with nanosized spherical shape has been synthesized through mechanochemical synthesis of calcium hydroxide and diammonium hydrogen phosphate. Sodium ion has been doped into HA by using sodium hydroxide precursor in a dry mixture of Ca(OH)2 and (NH3)2HPO4. Both Na-free HA and Na-doped HA (1% - 9%) are characterized by X-ray diffraction and Fourier transform infrared analyses. Reduction of the peak intensity and adsorption bands is observed with increasing Na+ concentration in the Na-doped HA structure. Increasing Na+ content expands the lattice parameters and unit cell volume of HA, while the crystallite size and degree of crystallinity decrease with increasing Na+ level. A mixture of rods and spheres are found in the Na+ doped HA. Characterization of the obtained powder suggests that Na doped HA has a potential to be used in clinical applications.
format	Article
author	Syed Abu Bakar, Sharifah Adzila Sopyan, Iis Singh, Ramesh Pusparini, Erlani
author_facet	Syed Abu Bakar, Sharifah Adzila Sopyan, Iis Singh, Ramesh Pusparini, Erlani
author_sort	Syed Abu Bakar, Sharifah Adzila
title	Mechanochemical synthesis of sodium doped hydroxyapatite powder
title_short	Mechanochemical synthesis of sodium doped hydroxyapatite powder
title_full	Mechanochemical synthesis of sodium doped hydroxyapatite powder
title_fullStr	Mechanochemical synthesis of sodium doped hydroxyapatite powder
title_full_unstemmed	Mechanochemical synthesis of sodium doped hydroxyapatite powder
title_sort	mechanochemical synthesis of sodium doped hydroxyapatite powder
publisher	Scientific Publishers of India
publishDate	2013
url	http://irep.iium.edu.my/31712/ http://irep.iium.edu.my/31712/ http://irep.iium.edu.my/31712/1/IJCA_52A%286%29_739-743.pdf
first_indexed	2023-09-18T20:45:52Z
last_indexed	2023-09-18T20:45:52Z
_version_	1777409670134104064

Mechanochemical synthesis of sodium doped hydroxyapatite powder

Similar Items