Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis

Methyl esters from vegetable oils have attracted a great deal of interest as substitute for petrodiesel to reduce dependence on imported petroleum and provide an alternate and sustainable source for fuel with more benign environmental properties. In the present study biodiesel was prepared from sunf...

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Main Authors:	Naureen, Rizwana, Tariq, Muhammad, Yusoff, Ismail, Khan Chowdhury, Ahmed Jalal, Ashraf, Muhammad Aqeel
Format:	Article
Language:	English English
Published:	ELSEVIER SCIENCE BV 2015
Subjects:	Q Science (General)
Online Access:	http://irep.iium.edu.my/43190/ http://irep.iium.edu.my/43190/ http://irep.iium.edu.my/43190/ http://irep.iium.edu.my/43190/1/biodiesel.pdf http://irep.iium.edu.my/43190/4/43190_Methanolysis_scopus.pdf

id	iium-43190
recordtype	eprints
spelling	iium-431902017-12-08T03:13:48Z http://irep.iium.edu.my/43190/ Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis Naureen, Rizwana Tariq, Muhammad Yusoff, Ismail Khan Chowdhury, Ahmed Jalal Ashraf, Muhammad Aqeel Q Science (General) Methyl esters from vegetable oils have attracted a great deal of interest as substitute for petrodiesel to reduce dependence on imported petroleum and provide an alternate and sustainable source for fuel with more benign environmental properties. In the present study biodiesel was prepared from sunflower seed oil by transesterification by alkali-catalyzed methanolysis. The fuel properties of sunflower oil biodiesel were determined and discussed in the light of ASTM D6751 standards for biodiesel. The sunflower oil biodiesel was chemically characterized with analytical techniques like FT-IR, and NMR (1H and 13C). The chemical composition of sunflower oil biodiesel was determined by GC–MS. Various fatty acid methyl esters (FAMEs) were identified by retention time data and verified by mass fragmentation patterns. The percentage conversion of triglycerides to the corresponding methyl esters determined by 1H NMR was 87.33% which was quite in good agreement with the practically observed yield of 85.1%. ELSEVIER SCIENCE BV 2015-05 Article PeerReviewed application/pdf en http://irep.iium.edu.my/43190/1/biodiesel.pdf application/pdf en http://irep.iium.edu.my/43190/4/43190_Methanolysis_scopus.pdf Naureen, Rizwana and Tariq, Muhammad and Yusoff, Ismail and Khan Chowdhury, Ahmed Jalal and Ashraf, Muhammad Aqeel (2015) Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis. Saudi Journal of Biological Sciences, 22 (3). pp. 332-339. ISSN 1319-562X http://www.sciencedirect.com/science/article/pii/S1319562X14001545 10.1016/j.sjbs.2014.11.017
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English English
topic	Q Science (General)
spellingShingle	Q Science (General) Naureen, Rizwana Tariq, Muhammad Yusoff, Ismail Khan Chowdhury, Ahmed Jalal Ashraf, Muhammad Aqeel Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis
description	Methyl esters from vegetable oils have attracted a great deal of interest as substitute for petrodiesel to reduce dependence on imported petroleum and provide an alternate and sustainable source for fuel with more benign environmental properties. In the present study biodiesel was prepared from sunflower seed oil by transesterification by alkali-catalyzed methanolysis. The fuel properties of sunflower oil biodiesel were determined and discussed in the light of ASTM D6751 standards for biodiesel. The sunflower oil biodiesel was chemically characterized with analytical techniques like FT-IR, and NMR (1H and 13C). The chemical composition of sunflower oil biodiesel was determined by GC–MS. Various fatty acid methyl esters (FAMEs) were identified by retention time data and verified by mass fragmentation patterns. The percentage conversion of triglycerides to the corresponding methyl esters determined by 1H NMR was 87.33% which was quite in good agreement with the practically observed yield of 85.1%.
format	Article
author	Naureen, Rizwana Tariq, Muhammad Yusoff, Ismail Khan Chowdhury, Ahmed Jalal Ashraf, Muhammad Aqeel
author_facet	Naureen, Rizwana Tariq, Muhammad Yusoff, Ismail Khan Chowdhury, Ahmed Jalal Ashraf, Muhammad Aqeel
author_sort	Naureen, Rizwana
title	Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis
title_short	Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis
title_full	Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis
title_fullStr	Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis
title_full_unstemmed	Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis
title_sort	synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis
publisher	ELSEVIER SCIENCE BV
publishDate	2015
url	http://irep.iium.edu.my/43190/ http://irep.iium.edu.my/43190/ http://irep.iium.edu.my/43190/ http://irep.iium.edu.my/43190/1/biodiesel.pdf http://irep.iium.edu.my/43190/4/43190_Methanolysis_scopus.pdf
first_indexed	2023-09-18T21:01:32Z
last_indexed	2023-09-18T21:01:32Z
_version_	1777410656576733184

Synthesis, spectroscopic and chromatographic studies of sunflower oil biodiesel using optimized base catalyzed methanolysis

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