2-[1-(2-Hydroxy-3-methoxybenzyl)-1H-benzimidazol-2-yl]-6-methoxyphenol methanol 1.13-solvate

In the main molecule of the title compound, C22H20N2O4·1.13CH4O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent molecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (...

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Bibliographic Details
Main Authors: Al-Douh, Mohammed H., Osman, Hasnah, Abd Hamid, Shafida, Kia, Reza, Fun, Hoong-Kun
Format: Article
Language:English
Published: International Union of Crystallography 2009
Subjects:
Online Access:http://irep.iium.edu.my/4369/
http://irep.iium.edu.my/4369/
http://irep.iium.edu.my/4369/
http://irep.iium.edu.my/4369/1/2-%5B1-%282-Hydr-oxy-3-methoxy-benz-yl%29.pdf
Description
Summary:In the main molecule of the title compound, C22H20N2O4·1.13CH4O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent molecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (5). The crystal structure is stabilized by intermolecular O-HO, O-HN and C-HO hydrogen bonds. The crystal studied was a merohedral twin [BASF ratio of 0.917 (1)/0.083 (1)].