Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics
Fracture toughness dependence of sintered hydroxyapatite (HA) bioceramics on the sintering time was studied. The nanocrystalline and highly pure Hydroxyapatite powders produced by wet chemical precipitation method were used as starting material. After uniaxial and cold isostatic pressing, the green...
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iium-46062013-06-27T02:51:20Z http://irep.iium.edu.my/4606/ Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics Tolouei, Ranna Singh, Ramesh Sopyan, Iis Yong, Tan Chou Amiriyan, Mahdi Dung, Teng Wan TA401 Materials of engineering and construction Fracture toughness dependence of sintered hydroxyapatite (HA) bioceramics on the sintering time was studied. The nanocrystalline and highly pure Hydroxyapatite powders produced by wet chemical precipitation method were used as starting material. After uniaxial and cold isostatic pressing, the green HA samples sintered at temperatures ranging from 1000 °C to 1300 °C with different sintering time. Dense compacts with grain sizes in the nanometer to micrometer range were processed. The average grain size of HA compact sintered at 1000 °C was around 500 nm. Grain size increased to 3 μm when the compacts were sintered at higher temperature. The average microhardness value of sintered HA decreased with an increased in grain size. Indentation fracture toughness for HA compacts of 700 nm grain size was 1.41±0.4 MPa.m1/2 which is similar to fracture toughness of human cortical bone. Trans Tech Publications 2011-07-27 Article PeerReviewed application/pdf en http://irep.iium.edu.my/4606/1/MSF_694_391.gif Tolouei, Ranna and Singh, Ramesh and Sopyan, Iis and Yong, Tan Chou and Amiriyan, Mahdi and Dung, Teng Wan (2011) Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics. Materials Science Forum, 694. pp. 391-395. ISSN 0255-5476 http://www.scientific.net/MSF.694.391 10.4028/www.scientific.net/MSF.694.391 |
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TA401 Materials of engineering and construction Tolouei, Ranna Singh, Ramesh Sopyan, Iis Yong, Tan Chou Amiriyan, Mahdi Dung, Teng Wan Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics |
description |
Fracture toughness dependence of sintered hydroxyapatite (HA) bioceramics on the sintering time was studied. The nanocrystalline and highly pure Hydroxyapatite powders produced by wet chemical precipitation method were used as starting material. After uniaxial and cold isostatic pressing, the green HA samples sintered at temperatures ranging from 1000 °C to 1300 °C with different sintering time. Dense compacts with grain sizes in the nanometer to micrometer range were processed. The average grain size of HA compact sintered at 1000 °C was around 500 nm. Grain size increased to 3 μm when the compacts were sintered at higher temperature. The average microhardness value of sintered HA decreased with an increased in grain size. Indentation fracture toughness for HA compacts of 700 nm grain size was 1.41±0.4 MPa.m1/2 which is similar to fracture toughness of human cortical bone. |
format |
Article |
author |
Tolouei, Ranna Singh, Ramesh Sopyan, Iis Yong, Tan Chou Amiriyan, Mahdi Dung, Teng Wan |
author_facet |
Tolouei, Ranna Singh, Ramesh Sopyan, Iis Yong, Tan Chou Amiriyan, Mahdi Dung, Teng Wan |
author_sort |
Tolouei, Ranna |
title |
Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics |
title_short |
Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics |
title_full |
Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics |
title_fullStr |
Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics |
title_full_unstemmed |
Dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics |
title_sort |
dependence of the fracture toughness on the sintering time of dense hydroxyapatite bioceramics |
publisher |
Trans Tech Publications |
publishDate |
2011 |
url |
http://irep.iium.edu.my/4606/ http://irep.iium.edu.my/4606/ http://irep.iium.edu.my/4606/ http://irep.iium.edu.my/4606/1/MSF_694_391.gif |
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2023-09-18T20:12:53Z |
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2023-09-18T20:12:53Z |
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