Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties

The influence of dispersant concentration on the physical properties of porous alumina ceramics formed by the protein foaming–consolidation method has been studied. Slurries of alumina powders, yolk, and dispersant were prepared by rigorously stirring the mixture for 3 h with an alumina-to-yolk ra...

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Main Authors: Ahmad, Fadli, Sopyan, Iis, Mel, Maizirwan, Ahmad, Zuraida
Format: Article
Language:English
English
Published: Curtin University of Technology and John Wiley & Sons, Ltd. 2011
Subjects:
Online Access:http://irep.iium.edu.my/4611/
http://irep.iium.edu.my/4611/
http://irep.iium.edu.my/4611/
http://irep.iium.edu.my/4611/1/APJCE_Fadli_published.pdf
http://irep.iium.edu.my/4611/4/Porous_alumina_through_protein_foaming2011.pdf
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spelling iium-46112013-07-02T08:31:48Z http://irep.iium.edu.my/4611/ Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties Ahmad, Fadli Sopyan, Iis Mel, Maizirwan Ahmad, Zuraida T Technology (General) The influence of dispersant concentration on the physical properties of porous alumina ceramics formed by the protein foaming–consolidation method has been studied. Slurries of alumina powders, yolk, and dispersant were prepared by rigorously stirring the mixture for 3 h with an alumina-to-yolk ratio of 1 : 1 in weight and dispersantconcentration of 0.01–0.05 wt.%. The resulting slip was poured into cylindrical shaped molds and followed by foamingand consolidation through drying at 180 ◦C for 1 h. The dried green bodies of the samples were then burned to remove the pore-creating agent at 600 ◦C for 1 h, followed by sintering at 1550 ◦C for 2 h. The density of sintered alumina ceramics could be controlled by varying the dispersant concentration of the slurry. Measurement of the average pore size distribution showed that macropores of the sintered alumina porous bodies increased with decreasing density and were found in the range of 54.4 ± 12 to 424.5 ± 25 μm. The compressive strength was 4.6 ± 0.8 MPa at 54.5% porosity and it decreased significantly to 0.8 ± 0.1 MPa at 71.8% porosity. A shrinkage of 29.3 ± 2.7% was observed for the sample prepared using the slurry without dispersant and it increased to 35.8 ± 0.9% when the dispersant of 0.03% was added. Curtin University of Technology and John Wiley & Sons, Ltd. 2011-01-16 Article PeerReviewed application/pdf en http://irep.iium.edu.my/4611/1/APJCE_Fadli_published.pdf application/pdf en http://irep.iium.edu.my/4611/4/Porous_alumina_through_protein_foaming2011.pdf Ahmad, Fadli and Sopyan, Iis and Mel, Maizirwan and Ahmad, Zuraida (2011) Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties. Asia-Pacific Journal of Chemical Engineering, 6. pp. 863-869. ISSN 1932-2143 http://onlinelibrary.wiley.com/journal/10.1002/%28ISSN%291932-2143 10.1002/apj.526
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
English
topic T Technology (General)
spellingShingle T Technology (General)
Ahmad, Fadli
Sopyan, Iis
Mel, Maizirwan
Ahmad, Zuraida
Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties
description The influence of dispersant concentration on the physical properties of porous alumina ceramics formed by the protein foaming–consolidation method has been studied. Slurries of alumina powders, yolk, and dispersant were prepared by rigorously stirring the mixture for 3 h with an alumina-to-yolk ratio of 1 : 1 in weight and dispersantconcentration of 0.01–0.05 wt.%. The resulting slip was poured into cylindrical shaped molds and followed by foamingand consolidation through drying at 180 ◦C for 1 h. The dried green bodies of the samples were then burned to remove the pore-creating agent at 600 ◦C for 1 h, followed by sintering at 1550 ◦C for 2 h. The density of sintered alumina ceramics could be controlled by varying the dispersant concentration of the slurry. Measurement of the average pore size distribution showed that macropores of the sintered alumina porous bodies increased with decreasing density and were found in the range of 54.4 ± 12 to 424.5 ± 25 μm. The compressive strength was 4.6 ± 0.8 MPa at 54.5% porosity and it decreased significantly to 0.8 ± 0.1 MPa at 71.8% porosity. A shrinkage of 29.3 ± 2.7% was observed for the sample prepared using the slurry without dispersant and it increased to 35.8 ± 0.9% when the dispersant of 0.03% was added.
format Article
author Ahmad, Fadli
Sopyan, Iis
Mel, Maizirwan
Ahmad, Zuraida
author_facet Ahmad, Fadli
Sopyan, Iis
Mel, Maizirwan
Ahmad, Zuraida
author_sort Ahmad, Fadli
title Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties
title_short Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties
title_full Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties
title_fullStr Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties
title_full_unstemmed Porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties
title_sort porous alumina through protein foaming–consolidation method: effect of dispersant concentration on the physical properties
publisher Curtin University of Technology and John Wiley & Sons, Ltd.
publishDate 2011
url http://irep.iium.edu.my/4611/
http://irep.iium.edu.my/4611/
http://irep.iium.edu.my/4611/
http://irep.iium.edu.my/4611/1/APJCE_Fadli_published.pdf
http://irep.iium.edu.my/4611/4/Porous_alumina_through_protein_foaming2011.pdf
first_indexed 2023-09-18T20:12:53Z
last_indexed 2023-09-18T20:12:53Z
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