Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent

Calcium hydroxides (Ca(OH)2) nanostructures have been fabricated through simple facile solution based synthesis at different temperatures 35, 45 and 55°C repectively. Ethanol was utilized as a medium for reaction. The synthesized powder was characterized by Field Emission Scanning Electron Micros...

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Main Authors:	Mohd Daud, Farah Diana, Sreekantan, Srimala, Mohamed, Abdul Rahman
Format:	Article
Language:	English
Published:	Trans Tech Publications Ltd. 2013
Subjects:	QD Chemistry TA170 Environmental engineering TA401 Materials of engineering and construction
Online Access:	http://irep.iium.edu.my/46394/ http://irep.iium.edu.my/46394/ http://irep.iium.edu.my/46394/ http://irep.iium.edu.my/46394/1/Fabrication_of_Ca%28OH%292_Nanostructures_by_Facile_Solution_%E2%80%93_Based_synthesis_at_various_reaction_temperatures_as_CO2_adsorbent.pdf

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spelling	iium-463942016-02-16T06:05:48Z http://irep.iium.edu.my/46394/ Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent Mohd Daud, Farah Diana Sreekantan, Srimala Mohamed, Abdul Rahman QD Chemistry TA170 Environmental engineering TA401 Materials of engineering and construction Calcium hydroxides (Ca(OH)2) nanostructures have been fabricated through simple facile solution based synthesis at different temperatures 35, 45 and 55°C repectively. Ethanol was utilized as a medium for reaction. The synthesized powder was characterized by Field Emission Scanning Electron Microscope (FESEM SUPRA 35VP ZEISS), Fourier transform infrared (FTIR Perkin Elmer Spectrum One Spectrophotometer) and X-ray diffraction (XRD). Based on XRD analysis, the synthesis samples exhibited crystal hexagonal phase of Ca(OH)2. The crystallite size for powders prepared was between 17 nm to 31 nm. Short nanorod like structures was successfully obtained in 80 ml ethanol solution for entire temperatures. However, the length and diameter decreased with increased the reaction temperatures. Short nanorod synthesized at 55°C has small diameters and length compared at 35°C. Carbon dioxide (CO2) adsorption for synthesized powders was studied by simultaneous thermal analyzer (STA). Ca(OH)2 prepared at 35°C and 45°C in 80 ml ethanol showed CO2 adsorption capacity about 9.3 mmol/g and 9.7 mmol/g respectively. Trans Tech Publications Ltd. 2013-05 Article PeerReviewed application/pdf en http://irep.iium.edu.my/46394/1/Fabrication_of_Ca%28OH%292_Nanostructures_by_Facile_Solution_%E2%80%93_Based_synthesis_at_various_reaction_temperatures_as_CO2_adsorbent.pdf Mohd Daud, Farah Diana and Sreekantan, Srimala and Mohamed, Abdul Rahman (2013) Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent. Materials Science Forum, 756. pp. 175-181. ISSN 1662-9752 http://www.scientific.net/MSF.756.175 10.4028/www.scientific.net/MSF.756.175
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English
topic	QD Chemistry TA170 Environmental engineering TA401 Materials of engineering and construction
spellingShingle	QD Chemistry TA170 Environmental engineering TA401 Materials of engineering and construction Mohd Daud, Farah Diana Sreekantan, Srimala Mohamed, Abdul Rahman Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent
description	Calcium hydroxides (Ca(OH)2) nanostructures have been fabricated through simple facile solution based synthesis at different temperatures 35, 45 and 55°C repectively. Ethanol was utilized as a medium for reaction. The synthesized powder was characterized by Field Emission Scanning Electron Microscope (FESEM SUPRA 35VP ZEISS), Fourier transform infrared (FTIR Perkin Elmer Spectrum One Spectrophotometer) and X-ray diffraction (XRD). Based on XRD analysis, the synthesis samples exhibited crystal hexagonal phase of Ca(OH)2. The crystallite size for powders prepared was between 17 nm to 31 nm. Short nanorod like structures was successfully obtained in 80 ml ethanol solution for entire temperatures. However, the length and diameter decreased with increased the reaction temperatures. Short nanorod synthesized at 55°C has small diameters and length compared at 35°C. Carbon dioxide (CO2) adsorption for synthesized powders was studied by simultaneous thermal analyzer (STA). Ca(OH)2 prepared at 35°C and 45°C in 80 ml ethanol showed CO2 adsorption capacity about 9.3 mmol/g and 9.7 mmol/g respectively.
format	Article
author	Mohd Daud, Farah Diana Sreekantan, Srimala Mohamed, Abdul Rahman
author_facet	Mohd Daud, Farah Diana Sreekantan, Srimala Mohamed, Abdul Rahman
author_sort	Mohd Daud, Farah Diana
title	Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent
title_short	Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent
title_full	Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent
title_fullStr	Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent
title_full_unstemmed	Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent
title_sort	fabrication of ca(oh)2 nanostructures by facile solution – based synthesis at various reaction temperatures as co2 adsorbent
publisher	Trans Tech Publications Ltd.
publishDate	2013
url	http://irep.iium.edu.my/46394/ http://irep.iium.edu.my/46394/ http://irep.iium.edu.my/46394/ http://irep.iium.edu.my/46394/1/Fabrication_of_Ca%28OH%292_Nanostructures_by_Facile_Solution_%E2%80%93_Based_synthesis_at_various_reaction_temperatures_as_CO2_adsorbent.pdf
first_indexed	2023-09-18T21:06:03Z
last_indexed	2023-09-18T21:06:03Z
_version_	1777410939850588160

Fabrication of Ca(OH)2 nanostructures by facile solution – based synthesis at various reaction temperatures as CO2 adsorbent

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