Production of polymethyl methacrylate grafted biopolymer using potassium persulfate

The production of the biodegradable poly (methyl methacrylate) (PMMA) onto sago starch biopolymer (Starch-gPMMA) was carried out using potassium persulfate (PPS) as an initiator. PMMA was grafted onto starch using PPS as an initiator under nitrogen gas atmosphere. The maximum percentage of graftin...

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Bibliographic Details
Main Authors: Qudsieh, I. Y., Mirghani, Mohamed Elwathig Saeed, Matar, Saleh M., Alkhatib, Maan F., Kabbashi, Nassereldeen Ahmed
Format: Conference or Workshop Item
Language:English
Published: Kulliyah of Engineering, International Islamic University Malaysia 2016
Subjects:
Online Access:http://irep.iium.edu.my/51708/
http://irep.iium.edu.my/51708/
http://irep.iium.edu.my/51708/1/51708.pdf
Description
Summary:The production of the biodegradable poly (methyl methacrylate) (PMMA) onto sago starch biopolymer (Starch-gPMMA) was carried out using potassium persulfate (PPS) as an initiator. PMMA was grafted onto starch using PPS as an initiator under nitrogen gas atmosphere. The maximum percentage of grafting (%G) was determined to be 90%. The optimum conditions were as follows: reaction temperature: 500C, the amount of monomer: 47 m.moles, the amount of PPS: 1.82 m.moles, and reaction period: 1.5 hr. The copolymers produced were characterized by Fourier Transform Infrared Spectrophotometry (FTIR), The FTIR spectra of the copolymers clearly indicated the presence of characteristic peaks of PMMA and starch, which suggested that PMMA had been successfully grafted on the starch.