Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline

Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline

The reaction of benzyl o-vanillin 1 with ophenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-benzyloxy-3- methoxybenzylidene) benzeneamine 2. The intermediate 2 is isolated and obtained as single crystals and their structures were determined...

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Bibliographic Details
Main Authors: Al-Douh, Mohammed Hadi, Osman, Hasnah, Abd Hamid, Shafida
Format: Conference or Workshop Item
Language:English
Published: icic-bme 2009
Subjects:
QD Chemistry
Online Access:http://irep.iium.edu.my/5353/
http://irep.iium.edu.my/5353/2/IEEE_Proceedings-Mohammad%5B2extract%5D.pdf
id iium-5353
recordtype eprints
spelling iium-53532011-11-21T14:39:35Z http://irep.iium.edu.my/5353/ Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline Al-Douh, Mohammed Hadi Osman, Hasnah Abd Hamid, Shafida QD Chemistry The reaction of benzyl o-vanillin 1 with ophenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-benzyloxy-3- methoxybenzylidene) benzeneamine 2. The intermediate 2 is isolated and obtained as single crystals and their structures were determined and studied by x-ray crystallography. The complete assignments of 2 were made using FTIR, HRMS, 1D and 2D NMR including 13C, COSY, HMQC and HMBC in CDCl3 and will be discussed. icic-bme 2009 Conference or Workshop Item PeerReviewed application/pdf en http://irep.iium.edu.my/5353/2/IEEE_Proceedings-Mohammad%5B2extract%5D.pdf Al-Douh, Mohammed Hadi and Osman, Hasnah and Abd Hamid, Shafida (2009) Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline. In: International Conference on Instrumentation, Communications, Information Technology and Biomedical Engineering (ICICI-BME) 2009, 23-25 November 2009, Institut Teknologi Bandung, Indonesia.
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
topic QD Chemistry
spellingShingle QD Chemistry
Al-Douh, Mohammed Hadi
Osman, Hasnah
Abd Hamid, Shafida
Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline
description The reaction of benzyl o-vanillin 1 with ophenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-benzyloxy-3- methoxybenzylidene) benzeneamine 2. The intermediate 2 is isolated and obtained as single crystals and their structures were determined and studied by x-ray crystallography. The complete assignments of 2 were made using FTIR, HRMS, 1D and 2D NMR including 13C, COSY, HMQC and HMBC in CDCl3 and will be discussed.
format Conference or Workshop Item
author Al-Douh, Mohammed Hadi
Osman, Hasnah
Abd Hamid, Shafida
author_facet Al-Douh, Mohammed Hadi
Osman, Hasnah
Abd Hamid, Shafida
author_sort Al-Douh, Mohammed Hadi
title Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline
title_short Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline
title_full Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline
title_fullStr Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline
title_full_unstemmed Synthesis, NMR spectroscopy and crystal structures studies of novel 2-amino-N-(2-benzyloxy-3-methoxybenzylidene) aniline
title_sort synthesis, nmr spectroscopy and crystal structures studies of novel 2-amino-n-(2-benzyloxy-3-methoxybenzylidene) aniline
publisher icic-bme
publishDate 2009
url http://irep.iium.edu.my/5353/
http://irep.iium.edu.my/5353/2/IEEE_Proceedings-Mohammad%5B2extract%5D.pdf
first_indexed 2023-09-18T20:13:53Z
last_indexed 2023-09-18T20:13:53Z
_version_ 1777407658619305984

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