Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline

The reaction of o–vanillin 1 with o-phenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline 2. Intermediate 2 is isolated and obtained as single crystals and the structure was determined and studied by x-ray cr...

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Main Authors:	Al-Douh, Mohammed Hadi, Osman, Hasnah, Abd Hamid, Shafida
Format:	Conference or Workshop Item
Language:	English
Published:	2009
Subjects:	QD Chemistry
Online Access:	http://irep.iium.edu.my/5354/ http://irep.iium.edu.my/5354/ http://irep.iium.edu.my/5354/2/IEEE_Proceedings-Mohammad%5B1extract%5D.pdf

id	iium-5354
recordtype	eprints
spelling	iium-53542011-12-23T07:00:28Z http://irep.iium.edu.my/5354/ Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline Al-Douh, Mohammed Hadi Osman, Hasnah Abd Hamid, Shafida QD Chemistry The reaction of o–vanillin 1 with o-phenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline 2. Intermediate 2 is isolated and obtained as single crystals and the structure was determined and studied by x-ray crystallography. The complete assignments of 2 were made using FTIR, HRMS, 1D and 2D NMR including APT, COSY, HMQC and HMBC in CDCl3 and will be discussed. 2009 Conference or Workshop Item PeerReviewed application/pdf en http://irep.iium.edu.my/5354/2/IEEE_Proceedings-Mohammad%5B1extract%5D.pdf Al-Douh, Mohammed Hadi and Osman, Hasnah and Abd Hamid, Shafida (2009) Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline. In: International Conference on Instrumentation, Communications, Information Technology, and Biomedical Engineering (ICICI-BME) 2009, 23-25 Nov 2009 , Bandung, Indonesia. http://ieeexplore.ieee.org/xpls/abs_all.jsp?arnumber=5417219
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English
topic	QD Chemistry
spellingShingle	QD Chemistry Al-Douh, Mohammed Hadi Osman, Hasnah Abd Hamid, Shafida Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline
description	The reaction of o–vanillin 1 with o-phenylenediamine 2PD, in dichloromethane at low conditions produced novel amino benzeneamine: 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline 2. Intermediate 2 is isolated and obtained as single crystals and the structure was determined and studied by x-ray crystallography. The complete assignments of 2 were made using FTIR, HRMS, 1D and 2D NMR including APT, COSY, HMQC and HMBC in CDCl3 and will be discussed.
format	Conference or Workshop Item
author	Al-Douh, Mohammed Hadi Osman, Hasnah Abd Hamid, Shafida
author_facet	Al-Douh, Mohammed Hadi Osman, Hasnah Abd Hamid, Shafida
author_sort	Al-Douh, Mohammed Hadi
title	Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline
title_short	Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline
title_full	Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline
title_fullStr	Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline
title_full_unstemmed	Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline
title_sort	synthesis, nmr spectroscopy and crystal structures studies of 2-amino-n-(2-hydroxy-3-methoxybenzylidene) aniline
publishDate	2009
url	http://irep.iium.edu.my/5354/ http://irep.iium.edu.my/5354/ http://irep.iium.edu.my/5354/2/IEEE_Proceedings-Mohammad%5B1extract%5D.pdf
first_indexed	2023-09-18T20:13:53Z
last_indexed	2023-09-18T20:13:53Z
_version_	1777407658764009472

Synthesis, NMR spectroscopy and crystal structures studies of 2-amino-N-(2-hydroxy-3-methoxybenzylidene) aniline

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