Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)

The effect of powder-to-liquid ratio and addition of poly(ethylene glycol) on the antiwashout behavior of calcium phosphate cement has been investigated. Calcium hydroxide, Ca(OH)2, and diammonium hydrogen phosphate, (NH4)2HPO4, were used as precursors with distilled water as the solvent in the w...

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Main Authors: Hablee, Sufiamie, Sopyan, Iis, Mel, Maizirwan, Mohd. Salleh, Hamzah, Rahman, Mujibur
Format: Conference or Workshop Item
Language:English
English
English
Published: Institute of Physics Publishing 2018
Subjects:
Online Access:http://irep.iium.edu.my/62774/
http://irep.iium.edu.my/62774/
http://irep.iium.edu.my/62774/
http://irep.iium.edu.my/62774/1/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate.pdf
http://irep.iium.edu.my/62774/2/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_SCOPUS.pdf
http://irep.iium.edu.my/62774/13/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_WoS.pdf
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spelling iium-627742018-07-31T01:08:05Z http://irep.iium.edu.my/62774/ Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) Hablee, Sufiamie Sopyan, Iis Mel, Maizirwan Mohd. Salleh, Hamzah Rahman, Mujibur TA401 Materials of engineering and construction The effect of powder-to-liquid ratio and addition of poly(ethylene glycol) on the antiwashout behavior of calcium phosphate cement has been investigated. Calcium hydroxide, Ca(OH)2, and diammonium hydrogen phosphate, (NH4)2HPO4, were used as precursors with distilled water as the solvent in the wet chemical precipitation synthesis of hydroxyapatite powder. Cement paste was prepared by mixing the as-synthesized powder with distilled water at certain ratios, varied at 1.0, 1.3, 1.5 and 1.6. Poly(ethylene glycol) was added into distilled water, varied at 1, 2, 3, 4 and 5 wt% using the powder-to-liquid ratio of 1.3. The antiwashout properties of the cement has been investigated by soaking in Ringer’s solution for 3 and 7 days. The evolution of compressive strength of calcium phosphate cement before and after soaking have been determined. After 7 days soaking, the strength of the cement increased by 94.4%, 2.98%, 11.39% and 111.29% for powder-to-liquid ratios 1.0, 1.3, 1.5 and 1.6 respectively. The addition of poly(ethylene glycol) up to 3% shows an increase in strength after 7 days soaking, with 57.75%, 16.4% and 19.97% increase for 1, 2 and 3% poly(ethylene glycol) contents respectively. The calcium phosphate cement produced in this current study shows excellent antiwashout behavior since no cement dissolution happened and the compressive strength of the cement increased with soaking time throughout 7 days soaking in Ringer’s solution. Institute of Physics Publishing 2018 Conference or Workshop Item PeerReviewed application/pdf en http://irep.iium.edu.my/62774/1/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate.pdf application/pdf en http://irep.iium.edu.my/62774/2/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_SCOPUS.pdf application/pdf en http://irep.iium.edu.my/62774/13/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_WoS.pdf Hablee, Sufiamie and Sopyan, Iis and Mel, Maizirwan and Mohd. Salleh, Hamzah and Rahman, Mujibur (2018) Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol). In: International Conference on Advances in Manufacturing and Materials Engineering 2017 (ICAMME17), 8th-9th August 2017, Kuala Lumpur, Malaysia. http://iopscience.iop.org/article/10.1088/1757-899X/290/1/012075/meta 10.1088/1757-899X/290/1/012075
repository_type Digital Repository
institution_category Local University
institution International Islamic University Malaysia
building IIUM Repository
collection Online Access
language English
English
English
topic TA401 Materials of engineering and construction
spellingShingle TA401 Materials of engineering and construction
Hablee, Sufiamie
Sopyan, Iis
Mel, Maizirwan
Mohd. Salleh, Hamzah
Rahman, Mujibur
Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
description The effect of powder-to-liquid ratio and addition of poly(ethylene glycol) on the antiwashout behavior of calcium phosphate cement has been investigated. Calcium hydroxide, Ca(OH)2, and diammonium hydrogen phosphate, (NH4)2HPO4, were used as precursors with distilled water as the solvent in the wet chemical precipitation synthesis of hydroxyapatite powder. Cement paste was prepared by mixing the as-synthesized powder with distilled water at certain ratios, varied at 1.0, 1.3, 1.5 and 1.6. Poly(ethylene glycol) was added into distilled water, varied at 1, 2, 3, 4 and 5 wt% using the powder-to-liquid ratio of 1.3. The antiwashout properties of the cement has been investigated by soaking in Ringer’s solution for 3 and 7 days. The evolution of compressive strength of calcium phosphate cement before and after soaking have been determined. After 7 days soaking, the strength of the cement increased by 94.4%, 2.98%, 11.39% and 111.29% for powder-to-liquid ratios 1.0, 1.3, 1.5 and 1.6 respectively. The addition of poly(ethylene glycol) up to 3% shows an increase in strength after 7 days soaking, with 57.75%, 16.4% and 19.97% increase for 1, 2 and 3% poly(ethylene glycol) contents respectively. The calcium phosphate cement produced in this current study shows excellent antiwashout behavior since no cement dissolution happened and the compressive strength of the cement increased with soaking time throughout 7 days soaking in Ringer’s solution.
format Conference or Workshop Item
author Hablee, Sufiamie
Sopyan, Iis
Mel, Maizirwan
Mohd. Salleh, Hamzah
Rahman, Mujibur
author_facet Hablee, Sufiamie
Sopyan, Iis
Mel, Maizirwan
Mohd. Salleh, Hamzah
Rahman, Mujibur
author_sort Hablee, Sufiamie
title Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
title_short Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
title_full Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
title_fullStr Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
title_full_unstemmed Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
title_sort antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
publisher Institute of Physics Publishing
publishDate 2018
url http://irep.iium.edu.my/62774/
http://irep.iium.edu.my/62774/
http://irep.iium.edu.my/62774/
http://irep.iium.edu.my/62774/1/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate.pdf
http://irep.iium.edu.my/62774/2/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_SCOPUS.pdf
http://irep.iium.edu.my/62774/13/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_WoS.pdf
first_indexed 2023-09-18T21:28:56Z
last_indexed 2023-09-18T21:28:56Z
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