Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol)
The effect of powder-to-liquid ratio and addition of poly(ethylene glycol) on the antiwashout behavior of calcium phosphate cement has been investigated. Calcium hydroxide, Ca(OH)2, and diammonium hydrogen phosphate, (NH4)2HPO4, were used as precursors with distilled water as the solvent in the w...
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2018
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iium-627742018-07-31T01:08:05Z http://irep.iium.edu.my/62774/ Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) Hablee, Sufiamie Sopyan, Iis Mel, Maizirwan Mohd. Salleh, Hamzah Rahman, Mujibur TA401 Materials of engineering and construction The effect of powder-to-liquid ratio and addition of poly(ethylene glycol) on the antiwashout behavior of calcium phosphate cement has been investigated. Calcium hydroxide, Ca(OH)2, and diammonium hydrogen phosphate, (NH4)2HPO4, were used as precursors with distilled water as the solvent in the wet chemical precipitation synthesis of hydroxyapatite powder. Cement paste was prepared by mixing the as-synthesized powder with distilled water at certain ratios, varied at 1.0, 1.3, 1.5 and 1.6. Poly(ethylene glycol) was added into distilled water, varied at 1, 2, 3, 4 and 5 wt% using the powder-to-liquid ratio of 1.3. The antiwashout properties of the cement has been investigated by soaking in Ringer’s solution for 3 and 7 days. The evolution of compressive strength of calcium phosphate cement before and after soaking have been determined. After 7 days soaking, the strength of the cement increased by 94.4%, 2.98%, 11.39% and 111.29% for powder-to-liquid ratios 1.0, 1.3, 1.5 and 1.6 respectively. The addition of poly(ethylene glycol) up to 3% shows an increase in strength after 7 days soaking, with 57.75%, 16.4% and 19.97% increase for 1, 2 and 3% poly(ethylene glycol) contents respectively. The calcium phosphate cement produced in this current study shows excellent antiwashout behavior since no cement dissolution happened and the compressive strength of the cement increased with soaking time throughout 7 days soaking in Ringer’s solution. Institute of Physics Publishing 2018 Conference or Workshop Item PeerReviewed application/pdf en http://irep.iium.edu.my/62774/1/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate.pdf application/pdf en http://irep.iium.edu.my/62774/2/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_SCOPUS.pdf application/pdf en http://irep.iium.edu.my/62774/13/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_WoS.pdf Hablee, Sufiamie and Sopyan, Iis and Mel, Maizirwan and Mohd. Salleh, Hamzah and Rahman, Mujibur (2018) Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol). In: International Conference on Advances in Manufacturing and Materials Engineering 2017 (ICAMME17), 8th-9th August 2017, Kuala Lumpur, Malaysia. http://iopscience.iop.org/article/10.1088/1757-899X/290/1/012075/meta 10.1088/1757-899X/290/1/012075 |
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TA401 Materials of engineering and construction |
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TA401 Materials of engineering and construction Hablee, Sufiamie Sopyan, Iis Mel, Maizirwan Mohd. Salleh, Hamzah Rahman, Mujibur Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) |
description |
The effect of powder-to-liquid ratio and addition of poly(ethylene glycol) on the
antiwashout behavior of calcium phosphate cement has been investigated. Calcium hydroxide,
Ca(OH)2, and diammonium hydrogen phosphate, (NH4)2HPO4, were used as precursors with
distilled water as the solvent in the wet chemical precipitation synthesis of hydroxyapatite
powder. Cement paste was prepared by mixing the as-synthesized powder with distilled water
at certain ratios, varied at 1.0, 1.3, 1.5 and 1.6. Poly(ethylene glycol) was added into distilled
water, varied at 1, 2, 3, 4 and 5 wt% using the powder-to-liquid ratio of 1.3. The antiwashout
properties of the cement has been investigated by soaking in Ringer’s solution for 3 and 7 days.
The evolution of compressive strength of calcium phosphate cement before and after soaking
have been determined. After 7 days soaking, the strength of the cement increased by 94.4%,
2.98%, 11.39% and 111.29% for powder-to-liquid ratios 1.0, 1.3, 1.5 and 1.6 respectively. The
addition of poly(ethylene glycol) up to 3% shows an increase in strength after 7 days soaking,
with 57.75%, 16.4% and 19.97% increase for 1, 2 and 3% poly(ethylene glycol) contents
respectively. The calcium phosphate cement produced in this current study shows excellent
antiwashout behavior since no cement dissolution happened and the compressive strength of
the cement increased with soaking time throughout 7 days soaking in Ringer’s solution. |
format |
Conference or Workshop Item |
author |
Hablee, Sufiamie Sopyan, Iis Mel, Maizirwan Mohd. Salleh, Hamzah Rahman, Mujibur |
author_facet |
Hablee, Sufiamie Sopyan, Iis Mel, Maizirwan Mohd. Salleh, Hamzah Rahman, Mujibur |
author_sort |
Hablee, Sufiamie |
title |
Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) |
title_short |
Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) |
title_full |
Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) |
title_fullStr |
Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) |
title_full_unstemmed |
Antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) |
title_sort |
antiwashout behavior of calcium phosphate cement incorporated with poly(ethylene glycol) |
publisher |
Institute of Physics Publishing |
publishDate |
2018 |
url |
http://irep.iium.edu.my/62774/ http://irep.iium.edu.my/62774/ http://irep.iium.edu.my/62774/ http://irep.iium.edu.my/62774/1/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate.pdf http://irep.iium.edu.my/62774/2/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_SCOPUS.pdf http://irep.iium.edu.my/62774/13/62774_Antiwashout%20Behavior%20of%20Calcium%20Phosphate_WoS.pdf |
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2023-09-18T21:28:56Z |
last_indexed |
2023-09-18T21:28:56Z |
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