Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles

The Fe3O4 magnetic nanoparticles (MNPs) attached with S-quinolin-2-yl-methyl-dithiocarbazate (SQ2MDTC) have been developed, aiming to function as the heavy metal adsorbent. The surface of MNPs was first coated with (3- aminopropyl)triethoxysilane (APTES) as cross-linker and then SQ2MDTC was covale...

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Main Authors:	Abdul Rahman, Ahmad Jazmi, Miskam, Mazidatulakmam Akmam, How, Fiona Ni Foong
Format:	Conference or Workshop Item
Language:	English
Published:	2018
Subjects:	QD Chemistry
Online Access:	http://irep.iium.edu.my/68775/ http://irep.iium.edu.my/68775/ http://irep.iium.edu.my/68775/1/selection%20%281%29.pdf

id	iium-68775
recordtype	eprints
spelling	iium-687752019-01-04T03:31:21Z http://irep.iium.edu.my/68775/ Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles Abdul Rahman, Ahmad Jazmi Miskam, Mazidatulakmam Akmam How, Fiona Ni Foong QD Chemistry The Fe3O4 magnetic nanoparticles (MNPs) attached with S-quinolin-2-yl-methyl-dithiocarbazate (SQ2MDTC) have been developed, aiming to function as the heavy metal adsorbent. The surface of MNPs was first coated with (3- aminopropyl)triethoxysilane (APTES) as cross-linker and then SQ2MDTC was covalently incorporated to the coated MNPs. The structural and surface characteristics were investigated by Fourier transform infrared spectroscopy (FT-IR), CHNS elemental analysis, thermogravimetric analysis (TGA), x-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and Brunauer-Emmett-Teller (BET) analysis. The SQ2MDTC functionalized MNPs exhibited high adsorption affinity for aqueous Cu(II) and Pb(II) ions when analysed using inductively coupled plasma optical emission spectrometer (ICP-OES), resulting from complexation of the metal ions by surface amino groups. Findings of the present work highlighted the potential of MNPSQ2MDTC as an effective adsorbent for the removal of heavy metal ions in water and wastewater treatment. 2018-08-17 Conference or Workshop Item PeerReviewed application/pdf en http://irep.iium.edu.my/68775/1/selection%20%281%29.pdf Abdul Rahman, Ahmad Jazmi and Miskam, Mazidatulakmam Akmam and How, Fiona Ni Foong (2018) Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles. In: International Conference of Analytical Sciences 2018 (SKAM 31), 17th-19th August 2018, Kuantan, Pahang. (Unpublished) http://www.iium.edu.my/skam31/
repository_type	Digital Repository
institution_category	Local University
institution	International Islamic University Malaysia
building	IIUM Repository
collection	Online Access
language	English
topic	QD Chemistry
spellingShingle	QD Chemistry Abdul Rahman, Ahmad Jazmi Miskam, Mazidatulakmam Akmam How, Fiona Ni Foong Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
description	The Fe3O4 magnetic nanoparticles (MNPs) attached with S-quinolin-2-yl-methyl-dithiocarbazate (SQ2MDTC) have been developed, aiming to function as the heavy metal adsorbent. The surface of MNPs was first coated with (3- aminopropyl)triethoxysilane (APTES) as cross-linker and then SQ2MDTC was covalently incorporated to the coated MNPs. The structural and surface characteristics were investigated by Fourier transform infrared spectroscopy (FT-IR), CHNS elemental analysis, thermogravimetric analysis (TGA), x-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and Brunauer-Emmett-Teller (BET) analysis. The SQ2MDTC functionalized MNPs exhibited high adsorption affinity for aqueous Cu(II) and Pb(II) ions when analysed using inductively coupled plasma optical emission spectrometer (ICP-OES), resulting from complexation of the metal ions by surface amino groups. Findings of the present work highlighted the potential of MNPSQ2MDTC as an effective adsorbent for the removal of heavy metal ions in water and wastewater treatment.
format	Conference or Workshop Item
author	Abdul Rahman, Ahmad Jazmi Miskam, Mazidatulakmam Akmam How, Fiona Ni Foong
author_facet	Abdul Rahman, Ahmad Jazmi Miskam, Mazidatulakmam Akmam How, Fiona Ni Foong
author_sort	Abdul Rahman, Ahmad Jazmi
title	Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_short	Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_full	Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_fullStr	Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_full_unstemmed	Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_sort	preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
publishDate	2018
url	http://irep.iium.edu.my/68775/ http://irep.iium.edu.my/68775/ http://irep.iium.edu.my/68775/1/selection%20%281%29.pdf
first_indexed	2023-09-18T21:37:34Z
last_indexed	2023-09-18T21:37:34Z
_version_	1777412923607482368

Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles

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