Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin

A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80...

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Main Authors:	Che Soh, Siti Kamilah, Jusoh, Siti Aminah, Shamsuddin, Mustaffa
Format:	Article
Language:	English
Published:	Research Management Institute (RMI) 2014
Subjects:	Palladium Polystyrene
Online Access:	http://ir.uitm.edu.my/id/eprint/12430/ http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf

id	uitm-12430
recordtype	eprints
spelling	uitm-124302016-05-26T02:46:51Z http://ir.uitm.edu.my/id/eprint/12430/ Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa Palladium Polystyrene A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy. Research Management Institute (RMI) 2014 Article PeerReviewed text en http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf Che Soh, Siti Kamilah and Jusoh, Siti Aminah and Shamsuddin, Mustaffa (2014) Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin. Scientific Research Journal, 11 (2). pp. 1-10. ISSN 1675-7009
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Teknologi MARA
building	UiTM Institutional Repository
collection	Online Access
language	English
topic	Palladium Polystyrene
spellingShingle	Palladium Polystyrene Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
description	A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy.
format	Article
author	Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa
author_facet	Che Soh, Siti Kamilah Jusoh, Siti Aminah Shamsuddin, Mustaffa
author_sort	Che Soh, Siti Kamilah
title	Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_short	Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_full	Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_fullStr	Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_full_unstemmed	Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin
title_sort	synthesis and physicochemical analysis of polystyrene-anchored pd(ii) metal complex / siti kamilah che soh, siti aminah jusoh and mustaffa shamsuddin
publisher	Research Management Institute (RMI)
publishDate	2014
url	http://ir.uitm.edu.my/id/eprint/12430/ http://ir.uitm.edu.my/id/eprint/12430/1/AJ_SITI%20KAMILAH%20CHE%20SOH%20SRJ%2014%201.pdf
first_indexed	2023-09-18T22:49:16Z
last_indexed	2023-09-18T22:49:16Z
_version_	1777417433799196672

Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin

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