Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]

Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]

This paper presents the application of Solid Phase Micro Extraction (SPME) coupled with Gas Chromatography-Mass Spectrometry (GC-MS) and Gas Chromatography-Flame Ionization Detector (GC-FID) to characterize agarwood incense. The work involved three types of SPME fibres at 30 minutes sampling time. T...

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Main Authors: Ismail, Nurlaila, Ibrahim, Mastura, Zareen, Seema, Rahiman, Mohd Hezri Fazalul, Tajuddin, Saiful Nizam, Taib, Mohd Nasir
Format: Article
Language:English
Published: Institute of Research Management and Innovation (IRMI) 2015
Subjects:
Extraction
Online Access:http://ir.uitm.edu.my/id/eprint/16086/
http://ir.uitm.edu.my/id/eprint/16086/1/AJ_NURLAILA%20ISMAIL%20SRJ%2015.pdf
id uitm-16086
recordtype eprints
spelling uitm-160862017-02-02T07:10:00Z http://ir.uitm.edu.my/id/eprint/16086/ Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.] Ismail, Nurlaila Ibrahim, Mastura Zareen, Seema Rahiman, Mohd Hezri Fazalul Tajuddin, Saiful Nizam Taib, Mohd Nasir Extraction This paper presents the application of Solid Phase Micro Extraction (SPME) coupled with Gas Chromatography-Mass Spectrometry (GC-MS) and Gas Chromatography-Flame Ionization Detector (GC-FID) to characterize agarwood incense. The work involved three types of SPME fibres at 30 minutes sampling time. The fibres are 50/30 jum divinylbenzene-carboxenpolydimethysiloxane (DVB-CAR-PDMS), 65 jum polydi methylsiloxanedivinylbenzene (PDMS-DVB) and 85 jum carboxen-polydimethyl siloxane (CAR-PDMS). The results showed that among many compounds extracted by GC-MS coupled with SPME, six compounds were found significantly presence in high quality agarwood incense due to their high percentage area (%). They are (5-maaliene, ᵝ-elemol, ᵝ-selinene, 10-epi-y-eudesmol, agarospirol and caryophellene oxide. The finding offers a new approach for establishing the volatile profile of agarwood incense components which is beneficial for agarwood grading and discrimination. Institute of Research Management and Innovation (IRMI) 2015 Article PeerReviewed text en http://ir.uitm.edu.my/id/eprint/16086/1/AJ_NURLAILA%20ISMAIL%20SRJ%2015.pdf Ismail, Nurlaila and Ibrahim, Mastura and Zareen, Seema and Rahiman, Mohd Hezri Fazalul and Tajuddin, Saiful Nizam and Taib, Mohd Nasir (2015) Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]. Scientific Research Journal, 12 (2). pp. 68-81. ISSN 1675-7009
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
topic Extraction
spellingShingle Extraction
Ismail, Nurlaila
Ibrahim, Mastura
Zareen, Seema
Rahiman, Mohd Hezri Fazalul
Tajuddin, Saiful Nizam
Taib, Mohd Nasir
Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]
description This paper presents the application of Solid Phase Micro Extraction (SPME) coupled with Gas Chromatography-Mass Spectrometry (GC-MS) and Gas Chromatography-Flame Ionization Detector (GC-FID) to characterize agarwood incense. The work involved three types of SPME fibres at 30 minutes sampling time. The fibres are 50/30 jum divinylbenzene-carboxenpolydimethysiloxane (DVB-CAR-PDMS), 65 jum polydi methylsiloxanedivinylbenzene (PDMS-DVB) and 85 jum carboxen-polydimethyl siloxane (CAR-PDMS). The results showed that among many compounds extracted by GC-MS coupled with SPME, six compounds were found significantly presence in high quality agarwood incense due to their high percentage area (%). They are (5-maaliene, ᵝ-elemol, ᵝ-selinene, 10-epi-y-eudesmol, agarospirol and caryophellene oxide. The finding offers a new approach for establishing the volatile profile of agarwood incense components which is beneficial for agarwood grading and discrimination.
format Article
author Ismail, Nurlaila
Ibrahim, Mastura
Zareen, Seema
Rahiman, Mohd Hezri Fazalul
Tajuddin, Saiful Nizam
Taib, Mohd Nasir
author_facet Ismail, Nurlaila
Ibrahim, Mastura
Zareen, Seema
Rahiman, Mohd Hezri Fazalul
Tajuddin, Saiful Nizam
Taib, Mohd Nasir
author_sort Ismail, Nurlaila
title Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]
title_short Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]
title_full Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]
title_fullStr Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]
title_full_unstemmed Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]
title_sort characterization of agarwood incense using gas chromatography – mass spectrometry (gc-ms) coupled with solid phase micro extraction (spme) and gas chromatography - flame ionization detector (gc-fid) / nurlaila ismail … [et al.]
publisher Institute of Research Management and Innovation (IRMI)
publishDate 2015
url http://ir.uitm.edu.my/id/eprint/16086/
http://ir.uitm.edu.my/id/eprint/16086/1/AJ_NURLAILA%20ISMAIL%20SRJ%2015.pdf
first_indexed 2023-09-18T22:55:19Z
last_indexed 2023-09-18T22:55:19Z
_version_ 1777417814450110464

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