Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham

The chemical compounds form the roots of Derris elliptica were extracted and isolated by various chromatography methods. The isolated compounds were elucidated by the spectroscopic methods. Extractions of the roots of Derris elliptica (300g) were done by macerated in the chloroform. The extraction y...

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Main Author:	Tengku Sham, Tengku Muzzabfarrullah
Format:	Student Project
Language:	English
Published:	Faculty of Applied Sciences 2008
Subjects:	Extraction (Chemistry)
Online Access:	http://ir.uitm.edu.my/id/eprint/23184/ http://ir.uitm.edu.my/id/eprint/23184/1/PPb_TENGKU%20MUZZABFARULLAH%20TENGKU%20SHAM%20AS%2008_5.pdf

id	uitm-23184
recordtype	eprints
spelling	uitm-231842019-02-14T09:20:59Z http://ir.uitm.edu.my/id/eprint/23184/ Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham Tengku Sham, Tengku Muzzabfarrullah Extraction (Chemistry) The chemical compounds form the roots of Derris elliptica were extracted and isolated by various chromatography methods. The isolated compounds were elucidated by the spectroscopic methods. Extractions of the roots of Derris elliptica (300g) were done by macerated in the chloroform. The extraction yield crude extract 8.74g (0.03 % w/w) were isolated using the chromatography methods. Vacuum liquid chromatography (VLC) and Radial chromatography (RC) were used to isolate the crude extract. Thin layer chromatography (TLC) was used to identify the pure compounds. The isolated crude produce two compound were produce labeled DEI (16.7mg) and DE2 (14.1mg). The pure compound were elucidated by the spectroscopic method; Nuclear Magnetic Resonance (NMR), Gas Chromatography - Mass Spectrometry (GC-MS), UV spectroscopy and Fourier Transform Infrared (FTIR). From the comparison of the spectrums with the literature reviews, the compounds were identified. Compound DEI known as rotenone and compound DE2 known as 2\-hydroxy-r,2'-dihydrorotenone. Faculty of Applied Sciences 2008 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/23184/1/PPb_TENGKU%20MUZZABFARULLAH%20TENGKU%20SHAM%20AS%2008_5.pdf Tengku Sham, Tengku Muzzabfarrullah (2008) Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham. [Student Project] (Unpublished)
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Teknologi MARA
building	UiTM Institutional Repository
collection	Online Access
language	English
topic	Extraction (Chemistry)
spellingShingle	Extraction (Chemistry) Tengku Sham, Tengku Muzzabfarrullah Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
description	The chemical compounds form the roots of Derris elliptica were extracted and isolated by various chromatography methods. The isolated compounds were elucidated by the spectroscopic methods. Extractions of the roots of Derris elliptica (300g) were done by macerated in the chloroform. The extraction yield crude extract 8.74g (0.03 % w/w) were isolated using the chromatography methods. Vacuum liquid chromatography (VLC) and Radial chromatography (RC) were used to isolate the crude extract. Thin layer chromatography (TLC) was used to identify the pure compounds. The isolated crude produce two compound were produce labeled DEI (16.7mg) and DE2 (14.1mg). The pure compound were elucidated by the spectroscopic method; Nuclear Magnetic Resonance (NMR), Gas Chromatography - Mass Spectrometry (GC-MS), UV spectroscopy and Fourier Transform Infrared (FTIR). From the comparison of the spectrums with the literature reviews, the compounds were identified. Compound DEI known as rotenone and compound DE2 known as 2\-hydroxy-r,2'-dihydrorotenone.
format	Student Project
author	Tengku Sham, Tengku Muzzabfarrullah
author_facet	Tengku Sham, Tengku Muzzabfarrullah
author_sort	Tengku Sham, Tengku Muzzabfarrullah
title	Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_short	Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_full	Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_fullStr	Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_full_unstemmed	Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham
title_sort	extraction and elucidation of chemical constituents from the roots of derris elliptic a / tengku muzzabfarrullah tengku sham
publisher	Faculty of Applied Sciences
publishDate	2008
url	http://ir.uitm.edu.my/id/eprint/23184/ http://ir.uitm.edu.my/id/eprint/23184/1/PPb_TENGKU%20MUZZABFARULLAH%20TENGKU%20SHAM%20AS%2008_5.pdf
first_indexed	2023-09-18T23:10:15Z
last_indexed	2023-09-18T23:10:15Z
_version_	1777418754223767552

Extraction and elucidation of chemical constituents from the roots of Derris Elliptic A / Tengku Muzzabfarrullah Tengku Sham

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