Determination of ascorbic acid in the multivitamin by differential pulse anodic stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari
Ascorbic acid cannot be synthesized by humans. This vitamin is rich in the varieties of vegetables and fruits. Nowadays, ascorbic acid has been transformed into multivitamin tablet which well-known as the dietary supplement. Growth in number of multivitamin tablet production increases curiosity a...
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| Format: | Student Project |
| Language: | English |
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Faculty of Applied Sciences
2017
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| Online Access: | http://ir.uitm.edu.my/id/eprint/24053/ http://ir.uitm.edu.my/id/eprint/24053/1/PPb_SITI%20NORBAITINA%20SHAARI%20AS%20C%2017_5.PDF |
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uitm-24053 |
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eprints |
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uitm-240532019-05-06T06:55:05Z http://ir.uitm.edu.my/id/eprint/24053/ Determination of ascorbic acid in the multivitamin by differential pulse anodic stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari Shaari, Siti Norbaitina Analytical chemistry Ascorbic acid cannot be synthesized by humans. This vitamin is rich in the varieties of vegetables and fruits. Nowadays, ascorbic acid has been transformed into multivitamin tablet which well-known as the dietary supplement. Growth in number of multivitamin tablet production increases curiosity among the researcher whether the content of ascorbic acid in the multivitamins dosage are in accordance with the standards and are safe to use by consumer. The differential pulse anodic stripping voltammetry (DPASV) technique using glassy carbon electrode (GCE) as the working electrode and phosphate buffer at pH 4.2 as the supporting electrolyte has been proposed to be developed. The experimental voltammetric parameters were optimized in order to obtain a maximum response with analytical validation of the technique. The optimum instrumental conditions for electroanalytical determination of ascorbic acid by the proposed DPASV technique were initial potential (Ei) = 0 V, final potential (Ef) = 0.7 V, accumulation time (tacc) = 60 s, scan rate (v) = 0.125 VIs, accumulation potential (Eacc) = 0 V and pulse amplitude = 0.150 V. The curve was linear from 5 mg/L to 300 mg/L (R2=0.999) with detection limit of 0.25 mg/L. The precisions in terms of relative standard deviation (RSD) were 1.3%,0.5% and 0.06%, respectively on the same day precision. The recoveries achieved for ascorbic acid Faculty of Applied Sciences 2017 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/24053/1/PPb_SITI%20NORBAITINA%20SHAARI%20AS%20C%2017_5.PDF Shaari, Siti Norbaitina (2017) Determination of ascorbic acid in the multivitamin by differential pulse anodic stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari. [Student Project] (Unpublished) |
| repository_type |
Digital Repository |
| institution_category |
Local University |
| institution |
Universiti Teknologi MARA |
| building |
UiTM Institutional Repository |
| collection |
Online Access |
| language |
English |
| topic |
Analytical chemistry |
| spellingShingle |
Analytical chemistry Shaari, Siti Norbaitina Determination of ascorbic acid in the multivitamin by differential pulse anodic stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari |
| description |
Ascorbic acid cannot be synthesized by humans. This vitamin is rich in the varieties of
vegetables and fruits. Nowadays, ascorbic acid has been transformed into multivitamin
tablet which well-known as the dietary supplement. Growth in number of multivitamin
tablet production increases curiosity among the researcher whether the content of ascorbic
acid in the multivitamins dosage are in accordance with the standards and are safe to use
by consumer. The differential pulse anodic stripping voltammetry (DPASV) technique
using glassy carbon electrode (GCE) as the working electrode and phosphate buffer at pH
4.2 as the supporting electrolyte has been proposed to be developed. The experimental
voltammetric parameters were optimized in order to obtain a maximum response with
analytical validation of the technique. The optimum instrumental conditions for
electroanalytical determination of ascorbic acid by the proposed DPASV technique were
initial potential (Ei) = 0 V, final potential (Ef) = 0.7 V, accumulation time (tacc) = 60 s,
scan rate (v) = 0.125 VIs, accumulation potential (Eacc) = 0 V and pulse amplitude = 0.150
V. The curve was linear from 5 mg/L to 300 mg/L (R2=0.999) with detection limit of 0.25
mg/L. The precisions in terms of relative standard deviation (RSD) were 1.3%,0.5% and
0.06%, respectively on the same day precision. The recoveries achieved for ascorbic acid |
| format |
Student Project |
| author |
Shaari, Siti Norbaitina |
| author_facet |
Shaari, Siti Norbaitina |
| author_sort |
Shaari, Siti Norbaitina |
| title |
Determination of ascorbic acid in the multivitamin by differential pulse anodic
stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari |
| title_short |
Determination of ascorbic acid in the multivitamin by differential pulse anodic
stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari |
| title_full |
Determination of ascorbic acid in the multivitamin by differential pulse anodic
stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari |
| title_fullStr |
Determination of ascorbic acid in the multivitamin by differential pulse anodic
stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari |
| title_full_unstemmed |
Determination of ascorbic acid in the multivitamin by differential pulse anodic
stripping voltammetric technique at a glassy carbon electrode / Siti Norbaitina Shaari |
| title_sort |
determination of ascorbic acid in the multivitamin by differential pulse anodic
stripping voltammetric technique at a glassy carbon electrode / siti norbaitina shaari |
| publisher |
Faculty of Applied Sciences |
| publishDate |
2017 |
| url |
http://ir.uitm.edu.my/id/eprint/24053/ http://ir.uitm.edu.my/id/eprint/24053/1/PPb_SITI%20NORBAITINA%20SHAARI%20AS%20C%2017_5.PDF |
| first_indexed |
2023-09-18T23:11:48Z |
| last_indexed |
2023-09-18T23:11:48Z |
| _version_ |
1777418851547348992 |