Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin

Gas Chromatography Flame Ionisation Detector (GC-FID) has been used in this study to determine the optimum initial oven temperature and carrier gas flow rate using three different Organophosphorus pesticides (OPPs) namely as vinclozolin, malathion and methidathion. A non-polar of HP-5 column was use...

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Main Author: Jamalludin, Imran Hakimie
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2016
Subjects:
Online Access:http://ir.uitm.edu.my/id/eprint/24268/
http://ir.uitm.edu.my/id/eprint/24268/1/PPb_IMRAN%20HAKIMIE%20JAMALLUDIN%20AS%20N%2016_5.pdf
id uitm-24268
recordtype eprints
spelling uitm-242682019-05-23T07:55:51Z http://ir.uitm.edu.my/id/eprint/24268/ Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin Jamalludin, Imran Hakimie QD Chemistry Gas Chromatography Flame Ionisation Detector (GC-FID) has been used in this study to determine the optimum initial oven temperature and carrier gas flow rate using three different Organophosphorus pesticides (OPPs) namely as vinclozolin, malathion and methidathion. A non-polar of HP-5 column was used as the injector and detector temperature were both set at 300°C using 1 μL injection volume. The initial oven temperature and carrier gas flow rate were ranged from 60°C to 110°C and 2 mL min-1 to 6 mL min-1 respectively. In the determination of the optimuminitial oven temperature and carrier gas flow rate, 90°C and 5 mL min-1 of theinitial oven temperature and carrier gas flow rate were fixed respectively. For the study on the effect of isothermal temperature, the temperatures were ranged from 150°C to 270°C. In this study, 90°C and 5 were chosen as the optimum initial oven temperature and carrier gas flow rate respectively as it based on the highest percentage of peak area of the pesticides. For the effect of isothermal temperature, 150°C, 180°C and 210°C were chosen as the best temperature as it showed highest in percentage of peak area for vinclozolin, malathion and methidathion respectively. Faculty of Applied Sciences 2016 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/24268/1/PPb_IMRAN%20HAKIMIE%20JAMALLUDIN%20AS%20N%2016_5.pdf Jamalludin, Imran Hakimie (2016) Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin. [Student Project] (Unpublished)
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
topic QD Chemistry
spellingShingle QD Chemistry
Jamalludin, Imran Hakimie
Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin
description Gas Chromatography Flame Ionisation Detector (GC-FID) has been used in this study to determine the optimum initial oven temperature and carrier gas flow rate using three different Organophosphorus pesticides (OPPs) namely as vinclozolin, malathion and methidathion. A non-polar of HP-5 column was used as the injector and detector temperature were both set at 300°C using 1 μL injection volume. The initial oven temperature and carrier gas flow rate were ranged from 60°C to 110°C and 2 mL min-1 to 6 mL min-1 respectively. In the determination of the optimuminitial oven temperature and carrier gas flow rate, 90°C and 5 mL min-1 of theinitial oven temperature and carrier gas flow rate were fixed respectively. For the study on the effect of isothermal temperature, the temperatures were ranged from 150°C to 270°C. In this study, 90°C and 5 were chosen as the optimum initial oven temperature and carrier gas flow rate respectively as it based on the highest percentage of peak area of the pesticides. For the effect of isothermal temperature, 150°C, 180°C and 210°C were chosen as the best temperature as it showed highest in percentage of peak area for vinclozolin, malathion and methidathion respectively.
format Student Project
author Jamalludin, Imran Hakimie
author_facet Jamalludin, Imran Hakimie
author_sort Jamalludin, Imran Hakimie
title Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin
title_short Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin
title_full Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin
title_fullStr Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin
title_full_unstemmed Study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / Imran Hakimie Jamalludin
title_sort study on the flow rate and initial oven temperature of gc-fid using pesticide analysis / imran hakimie jamalludin
publisher Faculty of Applied Sciences
publishDate 2016
url http://ir.uitm.edu.my/id/eprint/24268/
http://ir.uitm.edu.my/id/eprint/24268/1/PPb_IMRAN%20HAKIMIE%20JAMALLUDIN%20AS%20N%2016_5.pdf
first_indexed 2023-09-18T23:12:14Z
last_indexed 2023-09-18T23:12:14Z
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