Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah

Silica nanoparticles were prepared by Stober method using tetraethoxysilane as precursor, and ammonia as catalyst- The silica nanoparticles then were functionalized with silane coupling agent, 3-aminotriethoxysilane (APTES) to show the feasibility of anchoring functional group NH2 on silica nanop...

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Main Author: Rosdiansah, Siti Nurul Nadia
Format: Student Project
Language:English
Published: Faculty of Applied Sciences 2018
Subjects:
Online Access:http://ir.uitm.edu.my/id/eprint/24917/
http://ir.uitm.edu.my/id/eprint/24917/1/PPb_SITI%20NURUL%20NADIA%20ROSDIANSAH%20AS%20C%2018_5.PDF
id uitm-24917
recordtype eprints
spelling uitm-249172019-07-15T08:17:20Z http://ir.uitm.edu.my/id/eprint/24917/ Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah Rosdiansah, Siti Nurul Nadia Physical and theoretical chemistry Silica nanoparticles were prepared by Stober method using tetraethoxysilane as precursor, and ammonia as catalyst- The silica nanoparticles then were functionalized with silane coupling agent, 3-aminotriethoxysilane (APTES) to show the feasibility of anchoring functional group NH2 on silica nanoparticles surface. Five different concentration of ammonia was used to study the effect on the properties of silica nanoparticles. The samples were analyzed using SEM, XRD and FTIR. From the analysis, it has been found that the highest concentration of ammonia produced the largest particle size around 155.42 nm whereas the lowest concentration of ammonia produced the smallest particle size around 81.25 nm. The functionalization of APTES on the silica nanoparticles were analyzed using FTIR where the result shows the existence of amide group on the silica nanoparticles. This proves that the functionalization of APTES was successful. XRD pattern shows broad peak at 23° that defined as the typical amorphous state of silica. The reaction parameters should be optimized further to produce finer silica nanoparticles which has better solubility and more effective target drug delivery in biomedical field. Faculty of Applied Sciences 2018 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/24917/1/PPb_SITI%20NURUL%20NADIA%20ROSDIANSAH%20AS%20C%2018_5.PDF Rosdiansah, Siti Nurul Nadia (2018) Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah. [Student Project] (Unpublished)
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
topic Physical and theoretical chemistry
spellingShingle Physical and theoretical chemistry
Rosdiansah, Siti Nurul Nadia
Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah
description Silica nanoparticles were prepared by Stober method using tetraethoxysilane as precursor, and ammonia as catalyst- The silica nanoparticles then were functionalized with silane coupling agent, 3-aminotriethoxysilane (APTES) to show the feasibility of anchoring functional group NH2 on silica nanoparticles surface. Five different concentration of ammonia was used to study the effect on the properties of silica nanoparticles. The samples were analyzed using SEM, XRD and FTIR. From the analysis, it has been found that the highest concentration of ammonia produced the largest particle size around 155.42 nm whereas the lowest concentration of ammonia produced the smallest particle size around 81.25 nm. The functionalization of APTES on the silica nanoparticles were analyzed using FTIR where the result shows the existence of amide group on the silica nanoparticles. This proves that the functionalization of APTES was successful. XRD pattern shows broad peak at 23° that defined as the typical amorphous state of silica. The reaction parameters should be optimized further to produce finer silica nanoparticles which has better solubility and more effective target drug delivery in biomedical field.
format Student Project
author Rosdiansah, Siti Nurul Nadia
author_facet Rosdiansah, Siti Nurul Nadia
author_sort Rosdiansah, Siti Nurul Nadia
title Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah
title_short Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah
title_full Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah
title_fullStr Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah
title_full_unstemmed Effect of ammonia concentration on the properties of silica nanoparticles / Siti Nurul Nadia Rosdiansah
title_sort effect of ammonia concentration on the properties of silica nanoparticles / siti nurul nadia rosdiansah
publisher Faculty of Applied Sciences
publishDate 2018
url http://ir.uitm.edu.my/id/eprint/24917/
http://ir.uitm.edu.my/id/eprint/24917/1/PPb_SITI%20NURUL%20NADIA%20ROSDIANSAH%20AS%20C%2018_5.PDF
first_indexed 2023-09-18T23:13:39Z
last_indexed 2023-09-18T23:13:39Z
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