Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak

Volatile oil of Alpinia galanga species was extracted from young and old rhizome using ethyl acetate and hexane solution as extraction solvent. Alpinia galanga is one of the Zingiberaceae families in which it is very useful in treating disease and antimicrobial activities. Alpinia galanga is wide...

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Main Author: Ishak, Mohamad Adil Iman
Format: Student Project
Language:English
Published: Faculty Of Applied Sciences 2017
Subjects:
Online Access:http://ir.uitm.edu.my/id/eprint/25554/
http://ir.uitm.edu.my/id/eprint/25554/1/PPb_MOHAMAD%20ADIL%20IMAN%20ISHAK%20AS%20C%2017_5.PDF
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spelling uitm-255542019-09-19T08:28:00Z http://ir.uitm.edu.my/id/eprint/25554/ Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak Ishak, Mohamad Adil Iman Aromatic compounds Physical and theoretical chemistry Extraction (Chemistry) Volatile oil of Alpinia galanga species was extracted from young and old rhizome using ethyl acetate and hexane solution as extraction solvent. Alpinia galanga is one of the Zingiberaceae families in which it is very useful in treating disease and antimicrobial activities. Alpinia galanga is widely used in cooking, foods flavouring and perfumes production as it has nice and fragrance smell. Volatile oil was extracted from the young and old rhizome of Alpinia galanga by using hydro-distillation technique. The volatile oil obtained was extracted by using two different solvent solutions for each rhizome which was ethyl acetate and hexane solution. The volatile oil was then being analysed using Gas Chromatography Mass Spectroscopy (GC-MS) instrument. (S)-I-(4-acetoxyphenyl) propyl acetate compound was the main chemical constituent in the young rhizome volatile oil by using both types of solvent but different in percentage of similarity index. In ethyl acetate extraction solvent, this compound was detected in 95.3% of similarity index while in hexane extraction solvent, the compound was detected to be 93.9% of similarity index. In contrast, the main chemical compositions in the volatile oil of old rhizome of Alpinia galanga was (I S,4R,5R)-1 ,3,3-trimethyl-2 oxabicyclo [ 2.2.2] octan-5-yl acetate with 78.7% of similarity index for hexane solvent extraction and 95.9% for ethyl acetate solvent extraction. The data showed that ethyl acetate solvent had high efficiency in oil extraction compared to hexane solvent. Meanwhile, old rhizome yielded high amount of volatile oil compared to young rhizome of Alpinia galanga. Five new chemical constituents found in the volatile from both type of rhizomes were isopentyl acetate, 1,3,3-Trimethyl-2 oxabicyclo[ 2.2.2] oct-6-yl acetate, (S)-I-(4-Acetoxyphenyl) propyl acetate, (IS,4R,5R)-1 ,3,3-Trimethyl-2-oxabicyclo[2.2.2] octan-5-01 and (2S,2'S)-2,2'Bis [ I,4,7, I0, 13-pentaoxacyclopentadecane] since these compounds were not reported by any previous study. Faculty Of Applied Sciences 2017 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/25554/1/PPb_MOHAMAD%20ADIL%20IMAN%20ISHAK%20AS%20C%2017_5.PDF Ishak, Mohamad Adil Iman (2017) Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak. [Student Project] (Unpublished)
repository_type Digital Repository
institution_category Local University
institution Universiti Teknologi MARA
building UiTM Institutional Repository
collection Online Access
language English
topic Aromatic compounds
Physical and theoretical chemistry
Extraction (Chemistry)
spellingShingle Aromatic compounds
Physical and theoretical chemistry
Extraction (Chemistry)
Ishak, Mohamad Adil Iman
Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak
description Volatile oil of Alpinia galanga species was extracted from young and old rhizome using ethyl acetate and hexane solution as extraction solvent. Alpinia galanga is one of the Zingiberaceae families in which it is very useful in treating disease and antimicrobial activities. Alpinia galanga is widely used in cooking, foods flavouring and perfumes production as it has nice and fragrance smell. Volatile oil was extracted from the young and old rhizome of Alpinia galanga by using hydro-distillation technique. The volatile oil obtained was extracted by using two different solvent solutions for each rhizome which was ethyl acetate and hexane solution. The volatile oil was then being analysed using Gas Chromatography Mass Spectroscopy (GC-MS) instrument. (S)-I-(4-acetoxyphenyl) propyl acetate compound was the main chemical constituent in the young rhizome volatile oil by using both types of solvent but different in percentage of similarity index. In ethyl acetate extraction solvent, this compound was detected in 95.3% of similarity index while in hexane extraction solvent, the compound was detected to be 93.9% of similarity index. In contrast, the main chemical compositions in the volatile oil of old rhizome of Alpinia galanga was (I S,4R,5R)-1 ,3,3-trimethyl-2 oxabicyclo [ 2.2.2] octan-5-yl acetate with 78.7% of similarity index for hexane solvent extraction and 95.9% for ethyl acetate solvent extraction. The data showed that ethyl acetate solvent had high efficiency in oil extraction compared to hexane solvent. Meanwhile, old rhizome yielded high amount of volatile oil compared to young rhizome of Alpinia galanga. Five new chemical constituents found in the volatile from both type of rhizomes were isopentyl acetate, 1,3,3-Trimethyl-2 oxabicyclo[ 2.2.2] oct-6-yl acetate, (S)-I-(4-Acetoxyphenyl) propyl acetate, (IS,4R,5R)-1 ,3,3-Trimethyl-2-oxabicyclo[2.2.2] octan-5-01 and (2S,2'S)-2,2'Bis [ I,4,7, I0, 13-pentaoxacyclopentadecane] since these compounds were not reported by any previous study.
format Student Project
author Ishak, Mohamad Adil Iman
author_facet Ishak, Mohamad Adil Iman
author_sort Ishak, Mohamad Adil Iman
title Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak
title_short Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak
title_full Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak
title_fullStr Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak
title_full_unstemmed Chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / Mohamad Adil Iman Ishak
title_sort chemical composition of volatile oil of young and old rhizome of alpinia galanga plant / mohamad adil iman ishak
publisher Faculty Of Applied Sciences
publishDate 2017
url http://ir.uitm.edu.my/id/eprint/25554/
http://ir.uitm.edu.my/id/eprint/25554/1/PPb_MOHAMAD%20ADIL%20IMAN%20ISHAK%20AS%20C%2017_5.PDF
first_indexed 2023-09-18T23:14:58Z
last_indexed 2023-09-18T23:14:58Z
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