Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin

The graphite oxide and 2-methyl-4chlorophenoxy acetic acid- graphite oxide (MCPA-GO) nanocomposite were successfully synthesized by using improved Hummer's method and ion-exchange method respectively. In this study, MCPA-GO nanocomposite was synthesized at various concentration of MCP A rangin...

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Main Author:	Hasanuddin, Norilyani Izzati
Format:	Student Project
Language:	English
Published:	Faculty of Applied Sciences 2017
Subjects:	QD Chemistry Carbon disulfide. Graphene. Carbon
Online Access:	http://ir.uitm.edu.my/id/eprint/25584/ http://ir.uitm.edu.my/id/eprint/25584/1/PPb_NORILYANI%20IZZATI%20HASANUDDIN%20AS%20N%2017_5.pdf

id	uitm-25584
recordtype	eprints
spelling	uitm-255842019-09-26T00:34:53Z http://ir.uitm.edu.my/id/eprint/25584/ Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin Hasanuddin, Norilyani Izzati QD Chemistry Carbon disulfide. Graphene. Carbon The graphite oxide and 2-methyl-4chlorophenoxy acetic acid- graphite oxide (MCPA-GO) nanocomposite were successfully synthesized by using improved Hummer's method and ion-exchange method respectively. In this study, MCPA-GO nanocomposite was synthesized at various concentration of MCP A ranging from 0.1 to 0. 7 M to lowering its toxicity and increase the drugs/herbicides loading efficiency. Meanwhile, the graphite oxide was prepared with the use the graphite powder as starting material. Graphite oxide and MCPA-GO nanocomposite were characterized using Fourier transform infrared (FTIR) spectroscopy, powder X-ray diffraction (PXRD) and Carbon Hydrogen Nitrogen and Sulphur analyzer (CHNS). The FTIR spectra of MCPA-GO nanocomposite was showed resemblance peaks of the MCPA and graphite oxide indicated the inclusion of MCP A into the graphite oxide. As for XRD pattern, there was increasing in the basal spacing of the nanocomposite from the graphite oxide which by 9.3 A to 9.7 A. Other than that, the percentage loading of MCP A in the nanocomposite was calculated to be 98.0 % (w/w) based on the CHNS result. Next, the controlled release ofMCPA-GO nanocomposite was done in two different solution which were in sodium chloride solution (NaCl) and sodium carbonate solution (Na2CO3). The release of MCP A into these solution was found to be dependent to the anion in the order of Na2CO3 > NaCl with the percentage release of 66 % and 10 % respectively. It proved that this release property exhibits the potential application of graphite oxide as effective nanocarrier of herbicides. Faculty of Applied Sciences 2017 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/25584/1/PPb_NORILYANI%20IZZATI%20HASANUDDIN%20AS%20N%2017_5.pdf Hasanuddin, Norilyani Izzati (2017) Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin. [Student Project] (Unpublished)
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Teknologi MARA
building	UiTM Institutional Repository
collection	Online Access
language	English
topic	QD Chemistry Carbon disulfide. Graphene. Carbon
spellingShingle	QD Chemistry Carbon disulfide. Graphene. Carbon Hasanuddin, Norilyani Izzati Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin
description	The graphite oxide and 2-methyl-4chlorophenoxy acetic acid- graphite oxide (MCPA-GO) nanocomposite were successfully synthesized by using improved Hummer's method and ion-exchange method respectively. In this study, MCPA-GO nanocomposite was synthesized at various concentration of MCP A ranging from 0.1 to 0. 7 M to lowering its toxicity and increase the drugs/herbicides loading efficiency. Meanwhile, the graphite oxide was prepared with the use the graphite powder as starting material. Graphite oxide and MCPA-GO nanocomposite were characterized using Fourier transform infrared (FTIR) spectroscopy, powder X-ray diffraction (PXRD) and Carbon Hydrogen Nitrogen and Sulphur analyzer (CHNS). The FTIR spectra of MCPA-GO nanocomposite was showed resemblance peaks of the MCPA and graphite oxide indicated the inclusion of MCP A into the graphite oxide. As for XRD pattern, there was increasing in the basal spacing of the nanocomposite from the graphite oxide which by 9.3 A to 9.7 A. Other than that, the percentage loading of MCP A in the nanocomposite was calculated to be 98.0 % (w/w) based on the CHNS result. Next, the controlled release ofMCPA-GO nanocomposite was done in two different solution which were in sodium chloride solution (NaCl) and sodium carbonate solution (Na2CO3). The release of MCP A into these solution was found to be dependent to the anion in the order of Na2CO3 > NaCl with the percentage release of 66 % and 10 % respectively. It proved that this release property exhibits the potential application of graphite oxide as effective nanocarrier of herbicides.
format	Student Project
author	Hasanuddin, Norilyani Izzati
author_facet	Hasanuddin, Norilyani Izzati
author_sort	Hasanuddin, Norilyani Izzati
title	Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin
title_short	Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin
title_full	Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin
title_fullStr	Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin
title_full_unstemmed	Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin
title_sort	synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / norilyani izzati hasanuddin
publisher	Faculty of Applied Sciences
publishDate	2017
url	http://ir.uitm.edu.my/id/eprint/25584/ http://ir.uitm.edu.my/id/eprint/25584/1/PPb_NORILYANI%20IZZATI%20HASANUDDIN%20AS%20N%2017_5.pdf
first_indexed	2023-09-18T23:15:02Z
last_indexed	2023-09-18T23:15:02Z
_version_	1777419055008841728

Synthesis and characterization of graphite oxide and 2-methyl-4-chlorophenoxy acetic acidgraphite oxide (mcpa-go) nanocomposite with its controlled release property / Norilyani Izzati Hasanuddin

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