Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob
The main focus of this experiment was synthesizing 2,3-dioxopyrrolidine for the first part. There were three main reagents to achieve the first part of this experiment. The reagents were diethyl oxalate, methyl amine and aldehyde groups. The two different aldehyde groups used were anisaldehyde an...
| Main Author: | |
|---|---|
| Format: | Student Project |
| Language: | English |
| Published: |
Faculty of Applied Sciences
2009
|
| Subjects: | |
| Online Access: | http://ir.uitm.edu.my/id/eprint/495/ http://ir.uitm.edu.my/id/eprint/495/1/PPb_ISLAILI%20ULFAH%20YAAKOB%20AS%2009_5%20P01.pdf |
| id |
uitm-495 |
|---|---|
| recordtype |
eprints |
| spelling |
uitm-4952018-10-16T07:07:18Z http://ir.uitm.edu.my/id/eprint/495/ Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob Yaakob, Islaili Ulfah QD Chemistry The main focus of this experiment was synthesizing 2,3-dioxopyrrolidine for the first part. There were three main reagents to achieve the first part of this experiment. The reagents were diethyl oxalate, methyl amine and aldehyde groups. The two different aldehyde groups used were anisaldehyde and benzaldehyde. The structures of the 2,3-dioxopyrrolidine were determined using NMR. The second part of this experiment is decarboxylation. Each product from the first part underwent reflux for 2 hours in 10% HCl. The mixture obtained from decarboxylation was extracted with dicholomethane and ethyl acetate. The mixture then evaporated under reduced pressure. Faculty of Applied Sciences 2009 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/495/1/PPb_ISLAILI%20ULFAH%20YAAKOB%20AS%2009_5%20P01.pdf Yaakob, Islaili Ulfah (2009) Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob. [Student Project] (Unpublished) |
| repository_type |
Digital Repository |
| institution_category |
Local University |
| institution |
Universiti Teknologi MARA |
| building |
UiTM Institutional Repository |
| collection |
Online Access |
| language |
English |
| topic |
QD Chemistry |
| spellingShingle |
QD Chemistry Yaakob, Islaili Ulfah Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob |
| description |
The main focus of this experiment was synthesizing 2,3-dioxopyrrolidine for the first part. There
were three main reagents to achieve the first part of this experiment. The reagents were diethyl
oxalate, methyl amine and aldehyde groups. The two different aldehyde groups used were
anisaldehyde and benzaldehyde. The structures of the 2,3-dioxopyrrolidine were determined
using NMR. The second part of this experiment is decarboxylation. Each product from the first
part underwent reflux for 2 hours in 10% HCl. The mixture obtained from decarboxylation was
extracted with dicholomethane and ethyl acetate. The mixture then evaporated under reduced
pressure. |
| format |
Student Project |
| author |
Yaakob, Islaili Ulfah |
| author_facet |
Yaakob, Islaili Ulfah |
| author_sort |
Yaakob, Islaili Ulfah |
| title |
Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob |
| title_short |
Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob |
| title_full |
Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob |
| title_fullStr |
Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob |
| title_full_unstemmed |
Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob |
| title_sort |
synthesis and decarboxylation of 2-(4-methoxylphenyl)-1-methyl-4,5-dioxo-pyrollidine-3-carboxylic acid ethyl ester / islaili ulfah yaakob |
| publisher |
Faculty of Applied Sciences |
| publishDate |
2009 |
| url |
http://ir.uitm.edu.my/id/eprint/495/ http://ir.uitm.edu.my/id/eprint/495/1/PPb_ISLAILI%20ULFAH%20YAAKOB%20AS%2009_5%20P01.pdf |
| first_indexed |
2023-09-18T22:44:33Z |
| last_indexed |
2023-09-18T22:44:33Z |
| _version_ |
1777417137137123328 |