Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology

The aim of this work was to optimize equilibration temperature and time for analyzing volatiles components in palm sugar (Arenga pinnata) by headspace solid phase micro-extraction (HS-SPME) method. A 50/30 lm DVB/CAR/PDMS fiber was used to adsorb the volatile components from the headspace region. A...

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Main Authors:	Ho , Chun Wai, Wan Aida Wan Mustapha, Mohd. Yusof Maskat, Osman Hassan
Format:	Article
Published:	Universiti Kebangsaan Malaysia 2005
Online Access:	http://journalarticle.ukm.my/3944/ http://journalarticle.ukm.my/3944/

id	ukm-3944
recordtype	eprints
spelling	ukm-39442012-03-27T00:56:59Z http://journalarticle.ukm.my/3944/ Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology Ho , Chun Wai Wan Aida Wan Mustapha, Mohd. Yusof Maskat, Osman Hassan, The aim of this work was to optimize equilibration temperature and time for analyzing volatiles components in palm sugar (Arenga pinnata) by headspace solid phase micro-extraction (HS-SPME) method. A 50/30 lm DVB/CAR/PDMS fiber was used to adsorb the volatile components from the headspace region. A central composite statistical design was used to evaluate the effects of different temperatures (40 to 60°C) and sampling time (5 to 25 min) on the total yield of palm sugar volatile components. Response surfaces were plotted, and these together with results from some additional experiments (axial and center points) produced optimal extraction conditions for HS-SPME at 55°C and 12 min. These conditions were similar to N-heterocyclic compounds where the relative percentage area (RPA) was > 88.0% of total volatiles. Universiti Kebangsaan Malaysia 2005-12 Article PeerReviewed Ho , Chun Wai and Wan Aida Wan Mustapha, and Mohd. Yusof Maskat, and Osman Hassan, (2005) Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology. Sains Malaysiana, 34 (2). pp. 7-15. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol34num2_2005/vol34num2_05page7-15.html
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Kebangasaan Malaysia
building	UKM Institutional Repository
collection	Online Access
description	The aim of this work was to optimize equilibration temperature and time for analyzing volatiles components in palm sugar (Arenga pinnata) by headspace solid phase micro-extraction (HS-SPME) method. A 50/30 lm DVB/CAR/PDMS fiber was used to adsorb the volatile components from the headspace region. A central composite statistical design was used to evaluate the effects of different temperatures (40 to 60°C) and sampling time (5 to 25 min) on the total yield of palm sugar volatile components. Response surfaces were plotted, and these together with results from some additional experiments (axial and center points) produced optimal extraction conditions for HS-SPME at 55°C and 12 min. These conditions were similar to N-heterocyclic compounds where the relative percentage area (RPA) was > 88.0% of total volatiles.
format	Article
author	Ho , Chun Wai Wan Aida Wan Mustapha, Mohd. Yusof Maskat, Osman Hassan,
spellingShingle	Ho , Chun Wai Wan Aida Wan Mustapha, Mohd. Yusof Maskat, Osman Hassan, Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology
author_facet	Ho , Chun Wai Wan Aida Wan Mustapha, Mohd. Yusof Maskat, Osman Hassan,
author_sort	Ho , Chun Wai
title	Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology
title_short	Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology
title_full	Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology
title_fullStr	Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology
title_full_unstemmed	Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology
title_sort	optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology
publisher	Universiti Kebangsaan Malaysia
publishDate	2005
url	http://journalarticle.ukm.my/3944/ http://journalarticle.ukm.my/3944/
first_indexed	2023-09-18T19:40:13Z
last_indexed	2023-09-18T19:40:13Z
_version_	1777405540451745792

Optimization of headspace temperature and time sampling for identification of palm sugar volatile components using response surface methodology

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