Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups
Surface functionalization of multi-walled carbon nanotubes (MWCNTs) was carried out using a gas phase treatment in a Universal Temperature Program (UTP) reactor by flowing SO3 gas onto the CNTs while being heated at different temperatures. The functionalized nanotubes were characterized using X-ray...
| Main Authors: | , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Universiti Kebangsaan Malaysia
2012
|
| Online Access: | http://journalarticle.ukm.my/4474/ http://journalarticle.ukm.my/4474/ http://journalarticle.ukm.my/4474/1/12%2520Nuruzatulifah.pdf |
| id |
ukm-4474 |
|---|---|
| recordtype |
eprints |
| spelling |
ukm-44742016-12-14T06:36:07Z http://journalarticle.ukm.my/4474/ Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups Nuruzatulifah Asari @ Mansor, Tessonnier, Jean-Philippe Ali Rinaldi, Reiche, Sylvia M.G, Kutty Surface functionalization of multi-walled carbon nanotubes (MWCNTs) was carried out using a gas phase treatment in a Universal Temperature Program (UTP) reactor by flowing SO3 gas onto the CNTs while being heated at different temperatures. The functionalized nanotubes were characterized using X-ray Fluorescence (XRF), Fourier Transform Infrared Spectroscopy (FT-IR) and Raman spectroscopy. The amount of oxyen and sulfur containing groups was determined by acid-base titration. The titration results were in good agreement with elemental analysis using x-ray fluorescence. FTIR analysis showed the presence of oxygen and sulfur containing groups, S=O, C-S, C=O and -COOH. Raman spectroscopy confirmed that oxygen and sulfur containing acidic groups covalently attached to the sidewall of the MWCNTs. Universiti Kebangsaan Malaysia 2012-05 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/4474/1/12%2520Nuruzatulifah.pdf Nuruzatulifah Asari @ Mansor, and Tessonnier, Jean-Philippe and Ali Rinaldi, and Reiche, Sylvia and M.G, Kutty (2012) Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups. Sains Malaysiana, 41 (5). pp. 603-609. ISSN 0126-6039 http://www.ukm.my/jsm/ |
| repository_type |
Digital Repository |
| institution_category |
Local University |
| institution |
Universiti Kebangasaan Malaysia |
| building |
UKM Institutional Repository |
| collection |
Online Access |
| language |
English |
| description |
Surface functionalization of multi-walled carbon nanotubes (MWCNTs) was carried out using a gas phase treatment in a Universal Temperature Program (UTP) reactor by flowing SO3 gas onto the CNTs while being heated at different temperatures. The functionalized nanotubes were characterized using X-ray Fluorescence (XRF), Fourier Transform Infrared Spectroscopy (FT-IR) and Raman spectroscopy. The amount of oxyen and sulfur containing groups was determined by acid-base titration. The titration results were in good agreement with elemental analysis using x-ray fluorescence. FTIR analysis showed the presence of oxygen and sulfur containing groups, S=O, C-S, C=O and -COOH. Raman spectroscopy confirmed that oxygen and sulfur containing acidic groups covalently attached to the sidewall of the MWCNTs. |
| format |
Article |
| author |
Nuruzatulifah Asari @ Mansor, Tessonnier, Jean-Philippe Ali Rinaldi, Reiche, Sylvia M.G, Kutty |
| spellingShingle |
Nuruzatulifah Asari @ Mansor, Tessonnier, Jean-Philippe Ali Rinaldi, Reiche, Sylvia M.G, Kutty Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups |
| author_facet |
Nuruzatulifah Asari @ Mansor, Tessonnier, Jean-Philippe Ali Rinaldi, Reiche, Sylvia M.G, Kutty |
| author_sort |
Nuruzatulifah Asari @ Mansor, |
| title |
Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups |
| title_short |
Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups |
| title_full |
Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups |
| title_fullStr |
Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups |
| title_full_unstemmed |
Chemically Modified Multi-walled Carbon Nanotubes (MWCNTs) with Anchored Acidic Groups |
| title_sort |
chemically modified multi-walled carbon nanotubes (mwcnts) with anchored acidic groups |
| publisher |
Universiti Kebangsaan Malaysia |
| publishDate |
2012 |
| url |
http://journalarticle.ukm.my/4474/ http://journalarticle.ukm.my/4474/ http://journalarticle.ukm.my/4474/1/12%2520Nuruzatulifah.pdf |
| first_indexed |
2023-09-18T19:41:38Z |
| last_indexed |
2023-09-18T19:41:38Z |
| _version_ |
1777405629778886656 |