Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes

Titanate nanotubes were prepared by a rapid hydrothermal method in the presence of triethanolamine (TEA) using TiO2 nanoparticles as a precursor. The addition of TEA significantly reduced the formation time of the titanate nanotubes from 24 to 6 h. The crystalline structure of the titanate nanotubes...

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Main Authors: An'amt, M.N., Huang, N.M., Radiman, S., H.N., Lim, Muhamad, M.R.
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2014
Online Access:http://journalarticle.ukm.my/6826/
http://journalarticle.ukm.my/6826/
http://journalarticle.ukm.my/6826/1/18%2520M.N.%2520An%25D4%25C7%25D6amt.pdf
id ukm-6826
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spelling ukm-68262016-12-14T06:42:18Z http://journalarticle.ukm.my/6826/ Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes An'amt, M.N. Huang, N.M. Radiman, S. H.N., Lim Muhamad, M.R. Titanate nanotubes were prepared by a rapid hydrothermal method in the presence of triethanolamine (TEA) using TiO2 nanoparticles as a precursor. The addition of TEA significantly reduced the formation time of the titanate nanotubes from 24 to 6 h. The crystalline structure of the titanate nanotubes was revealed to be H2Ti2O5 through the X-ray diffraction (XRD) measurement. The morphology of the titanate nanotubes was confirmed using transmission electron microscopy (TEM) while the surface area was characterized using Brunauer-Emmett-Teller (BET) surface area analysis. The titanate nanotubes produced were several hundred nanometers in length and had an average outer diameter of ~ 11.5 nm, inner diameter of ~5.0 nm, interlayer spacing of 0.93 nm and surface area of >250 m2/g. The photocatalytic activity of the titanate nanotubes was studied using methylene blue as a model dye; the titanate nanotubes showed better photocatalytic performance as compared to TiO2 nanoparticles. Universiti Kebangsaan Malaysia 2014-01 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/6826/1/18%2520M.N.%2520An%25D4%25C7%25D6amt.pdf An'amt, M.N. and Huang, N.M. and Radiman, S. and H.N., Lim and Muhamad, M.R. (2014) Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes. Sains Malaysiana, 43 (1). pp. 137-144. ISSN 0126-6039 http://www.ukm.my/jsm/
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description Titanate nanotubes were prepared by a rapid hydrothermal method in the presence of triethanolamine (TEA) using TiO2 nanoparticles as a precursor. The addition of TEA significantly reduced the formation time of the titanate nanotubes from 24 to 6 h. The crystalline structure of the titanate nanotubes was revealed to be H2Ti2O5 through the X-ray diffraction (XRD) measurement. The morphology of the titanate nanotubes was confirmed using transmission electron microscopy (TEM) while the surface area was characterized using Brunauer-Emmett-Teller (BET) surface area analysis. The titanate nanotubes produced were several hundred nanometers in length and had an average outer diameter of ~ 11.5 nm, inner diameter of ~5.0 nm, interlayer spacing of 0.93 nm and surface area of >250 m2/g. The photocatalytic activity of the titanate nanotubes was studied using methylene blue as a model dye; the titanate nanotubes showed better photocatalytic performance as compared to TiO2 nanoparticles.
format Article
author An'amt, M.N.
Huang, N.M.
Radiman, S.
H.N., Lim
Muhamad, M.R.
spellingShingle An'amt, M.N.
Huang, N.M.
Radiman, S.
H.N., Lim
Muhamad, M.R.
Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes
author_facet An'amt, M.N.
Huang, N.M.
Radiman, S.
H.N., Lim
Muhamad, M.R.
author_sort An'amt, M.N.
title Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes
title_short Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes
title_full Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes
title_fullStr Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes
title_full_unstemmed Triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes
title_sort triethanolamine – solution for rapid hydrothermal synthesis of titanate nanotubes
publisher Universiti Kebangsaan Malaysia
publishDate 2014
url http://journalarticle.ukm.my/6826/
http://journalarticle.ukm.my/6826/
http://journalarticle.ukm.my/6826/1/18%2520M.N.%2520An%25D4%25C7%25D6amt.pdf
first_indexed 2023-09-18T19:48:00Z
last_indexed 2023-09-18T19:48:00Z
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