Preparation of transition metal sulfide nanoparticles via hydrothermal route

Nano sized copper sulfide, iron sulfide and molybdenum sulfide were successfully synthesised via a simple hydrothermal method. Sodium thiosulfate pentahydrate (Na2S2O3¥5H2O) and hydroxylamine sulfate ((H3NO)2¥H2SO4) were used as the starting materials and reacted with the transition metal source at...

Full description

Bibliographic Details
Main Authors:	Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang
Format:	Article
Language:	English
Published:	Universiti Kebangsaan Malaysia 2010
Online Access:	http://journalarticle.ukm.my/7326/ http://journalarticle.ukm.my/7326/ http://journalarticle.ukm.my/7326/1/01_Md_Yeaminhossain.pdf

id	ukm-7326
recordtype	eprints
spelling	ukm-73262016-12-14T06:43:45Z http://journalarticle.ukm.my/7326/ Preparation of transition metal sulfide nanoparticles via hydrothermal route Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang, Nano sized copper sulfide, iron sulfide and molybdenum sulfide were successfully synthesised via a simple hydrothermal method. Sodium thiosulfate pentahydrate (Na2S2O3¥5H2O) and hydroxylamine sulfate ((H3NO)2¥H2SO4) were used as the starting materials and reacted with the transition metal source at 200oC for 90 min. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX) and Fourier transform infrared spectroscopy (FTIR). Spherical shape CuS and FeS2 nanoparticles with high crystallinity were successfully produced. The transmission electron micrographs revealed the well-dispersibility of the produced nanoparticles. Scanning electron micrograph showed the MoS2 nanoparticles possessed a spherical shape with sheet-like structure covering on the outer surface of the particles. Universiti Kebangsaan Malaysia 2010-04 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/7326/1/01_Md_Yeaminhossain.pdf Fei-Ling Pua, and Chin-Hua Chia, and Sarani Zakaria, and Tze-Khong Liew, and Mohd Ambar Yarmo, and Nay-Ming Huang, (2010) Preparation of transition metal sulfide nanoparticles via hydrothermal route. Sains Malaysiana, 39 (2). pp. 243-248. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol39num2_2010/contentsVol39num2_2010.html
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Kebangasaan Malaysia
building	UKM Institutional Repository
collection	Online Access
language	English
description	Nano sized copper sulfide, iron sulfide and molybdenum sulfide were successfully synthesised via a simple hydrothermal method. Sodium thiosulfate pentahydrate (Na2S2O3¥5H2O) and hydroxylamine sulfate ((H3NO)2¥H2SO4) were used as the starting materials and reacted with the transition metal source at 200oC for 90 min. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX) and Fourier transform infrared spectroscopy (FTIR). Spherical shape CuS and FeS2 nanoparticles with high crystallinity were successfully produced. The transmission electron micrographs revealed the well-dispersibility of the produced nanoparticles. Scanning electron micrograph showed the MoS2 nanoparticles possessed a spherical shape with sheet-like structure covering on the outer surface of the particles.
format	Article
author	Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang,
spellingShingle	Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang, Preparation of transition metal sulfide nanoparticles via hydrothermal route
author_facet	Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang,
author_sort	Fei-Ling Pua,
title	Preparation of transition metal sulfide nanoparticles via hydrothermal route
title_short	Preparation of transition metal sulfide nanoparticles via hydrothermal route
title_full	Preparation of transition metal sulfide nanoparticles via hydrothermal route
title_fullStr	Preparation of transition metal sulfide nanoparticles via hydrothermal route
title_full_unstemmed	Preparation of transition metal sulfide nanoparticles via hydrothermal route
title_sort	preparation of transition metal sulfide nanoparticles via hydrothermal route
publisher	Universiti Kebangsaan Malaysia
publishDate	2010
url	http://journalarticle.ukm.my/7326/ http://journalarticle.ukm.my/7326/ http://journalarticle.ukm.my/7326/1/01_Md_Yeaminhossain.pdf
first_indexed	2023-09-18T19:49:23Z
last_indexed	2023-09-18T19:49:23Z
_version_	1777406116396793856

Preparation of transition metal sulfide nanoparticles via hydrothermal route

Similar Items