Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study

Ceramics powder of BaCe0.54Zr0.36Y0.1O2.95 (BCZY) was synthesized using three different methods namely sol-gel (SG), supercritical fluid (SC) and supercritical fluid assisted sol-gel (SCSG). The respective prepared samples were denoted as S1, S2 and S3. TG thermogram of the dried powders for all sam...

Full description

Bibliographic Details
Main Authors:	Nafisah Osman, Najwa ‘Adni Ibarahim, Mohd. Azlan Mohd. Ishak, Oskar Hasdinor Hassan
Format:	Article
Language:	English
Published:	Universiti Kebangsaan Malaysia 2014
Online Access:	http://journalarticle.ukm.my/7672/ http://journalarticle.ukm.my/7672/ http://journalarticle.ukm.my/7672/1/11_Nafisah_Osman.pdf

id	ukm-7672
recordtype	eprints
spelling	ukm-76722016-12-14T06:44:50Z http://journalarticle.ukm.my/7672/ Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study Nafisah Osman, Najwa ‘Adni Ibarahim, Mohd. Azlan Mohd. Ishak, Oskar Hasdinor Hassan, Ceramics powder of BaCe0.54Zr0.36Y0.1O2.95 (BCZY) was synthesized using three different methods namely sol-gel (SG), supercritical fluid (SC) and supercritical fluid assisted sol-gel (SCSG). The respective prepared samples were denoted as S1, S2 and S3. TG thermogram of the dried powders for all samples showed three stages of weight loss. Each stage was corroborated by one or two exothermic peaks as shown in DTG signal. Complete thermal decomposition for all the samples was almost accomplished at 1000°C for about 2 h. At calcination temperature of 1100°C, S1 showed a single-phase of perovskite-type oxides as proven by XRD result. Morphology of the calcined powders by SEM micrograph showed that S1 is in spherical shape, S2 is in cubic structure and S3 has a mixture of spherical and rod-like structure. Therefore, as comparison, SG method gives better characteristics of cerate-zirconate ceramics powder compared to SC and SGSC. Universiti Kebangsaan Malaysia 2014-09 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/7672/1/11_Nafisah_Osman.pdf Nafisah Osman, and Najwa ‘Adni Ibarahim, and Mohd. Azlan Mohd. Ishak, and Oskar Hasdinor Hassan, (2014) Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study. Sains Malaysiana, 43 (9). pp. 1373-1378. ISSN 0126-6039 http://www.ukm.my/jsm/
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Kebangasaan Malaysia
building	UKM Institutional Repository
collection	Online Access
language	English
description	Ceramics powder of BaCe0.54Zr0.36Y0.1O2.95 (BCZY) was synthesized using three different methods namely sol-gel (SG), supercritical fluid (SC) and supercritical fluid assisted sol-gel (SCSG). The respective prepared samples were denoted as S1, S2 and S3. TG thermogram of the dried powders for all samples showed three stages of weight loss. Each stage was corroborated by one or two exothermic peaks as shown in DTG signal. Complete thermal decomposition for all the samples was almost accomplished at 1000°C for about 2 h. At calcination temperature of 1100°C, S1 showed a single-phase of perovskite-type oxides as proven by XRD result. Morphology of the calcined powders by SEM micrograph showed that S1 is in spherical shape, S2 is in cubic structure and S3 has a mixture of spherical and rod-like structure. Therefore, as comparison, SG method gives better characteristics of cerate-zirconate ceramics powder compared to SC and SGSC.
format	Article
author	Nafisah Osman, Najwa ‘Adni Ibarahim, Mohd. Azlan Mohd. Ishak, Oskar Hasdinor Hassan,
spellingShingle	Nafisah Osman, Najwa ‘Adni Ibarahim, Mohd. Azlan Mohd. Ishak, Oskar Hasdinor Hassan, Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study
author_facet	Nafisah Osman, Najwa ‘Adni Ibarahim, Mohd. Azlan Mohd. Ishak, Oskar Hasdinor Hassan,
author_sort	Nafisah Osman,
title	Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study
title_short	Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study
title_full	Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study
title_fullStr	Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study
title_full_unstemmed	Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study
title_sort	characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study
publisher	Universiti Kebangsaan Malaysia
publishDate	2014
url	http://journalarticle.ukm.my/7672/ http://journalarticle.ukm.my/7672/ http://journalarticle.ukm.my/7672/1/11_Nafisah_Osman.pdf
first_indexed	2023-09-18T19:50:21Z
last_indexed	2023-09-18T19:50:21Z
_version_	1777406177436499968

Characterization of cerate-zirconate ceramics powder prepared by three different methods: a comparative study

Similar Items