Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method

Nanoparticles of Zn1-xFexS (x = 0.0, 0.1, 0.2 and 0.3) were prepared by chemical co-precipitation method from homogenous solution of zinc and ferum salt at room temperature with controlled parameter. These nanoparticles were sterically stabilized using Sodium Hexamethaphospate (SHMP). Here, a stud...

Full description

Bibliographic Details
Main Authors:	Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak
Format:	Article
Language:	English
Published:	Fakulti Kejuruteraan ,UKM,Bangi. 2015
Online Access:	http://journalarticle.ukm.my/9512/ http://journalarticle.ukm.my/9512/ http://journalarticle.ukm.my/9512/1/12.pdf

id	ukm-9512
recordtype	eprints
spelling	ukm-95122016-12-14T06:50:09Z http://journalarticle.ukm.my/9512/ Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak, Nanoparticles of Zn1-xFexS (x = 0.0, 0.1, 0.2 and 0.3) were prepared by chemical co-precipitation method from homogenous solution of zinc and ferum salt at room temperature with controlled parameter. These nanoparticles were sterically stabilized using Sodium Hexamethaphospate (SHMP). Here, a study of the effect of Fe doping on structure and optical properties of nanoparticles was undertaken. Structure, elemental analysis and optical properties have been investigated by X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM), Fourier-Transform-Infrared spectroscopy (FT-IR), X-Ray Fluorescence (XRF), UV-Visible Spectroscopy and photoluminescence (PL) spectrophotometer. FT-IR and XRF results confi rmed the incorporation of ion dopants into ZnS crystal structure, and XRD results showed that Zn1-xFexS (x = 0.00 and 0.10) nanoparticles crystallized in a zinc blende structure without any impurity. The particle size of all of samples ranged from 2 nm to 3 nm, as calculated by the Debye-Scherrer formula. The optical absorption spectra indicate a blue shift of the absorption edge with increasing Fe-content. The luminescence of nanoparticles excite at about 370 nm with an emission peak at around at 452 nm, 490 nm and 550 nm. Fakulti Kejuruteraan ,UKM,Bangi. 2015 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/9512/1/12.pdf Rahizana Mohd Ibrahim, and Masturah Markom, and Kamal Firdausi Abd Razak, (2015) Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method. Jurnal Kejuruteraan, 27 . pp. 87-94. ISSN 0128-0198 http://www.ukm.my/jkukm/?page_id=557
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Kebangasaan Malaysia
building	UKM Institutional Repository
collection	Online Access
language	English
description	Nanoparticles of Zn1-xFexS (x = 0.0, 0.1, 0.2 and 0.3) were prepared by chemical co-precipitation method from homogenous solution of zinc and ferum salt at room temperature with controlled parameter. These nanoparticles were sterically stabilized using Sodium Hexamethaphospate (SHMP). Here, a study of the effect of Fe doping on structure and optical properties of nanoparticles was undertaken. Structure, elemental analysis and optical properties have been investigated by X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM), Fourier-Transform-Infrared spectroscopy (FT-IR), X-Ray Fluorescence (XRF), UV-Visible Spectroscopy and photoluminescence (PL) spectrophotometer. FT-IR and XRF results confi rmed the incorporation of ion dopants into ZnS crystal structure, and XRD results showed that Zn1-xFexS (x = 0.00 and 0.10) nanoparticles crystallized in a zinc blende structure without any impurity. The particle size of all of samples ranged from 2 nm to 3 nm, as calculated by the Debye-Scherrer formula. The optical absorption spectra indicate a blue shift of the absorption edge with increasing Fe-content. The luminescence of nanoparticles excite at about 370 nm with an emission peak at around at 452 nm, 490 nm and 550 nm.
format	Article
author	Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak,
spellingShingle	Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak, Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method
author_facet	Rahizana Mohd Ibrahim, Masturah Markom, Kamal Firdausi Abd Razak,
author_sort	Rahizana Mohd Ibrahim,
title	Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method
title_short	Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method
title_full	Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method
title_fullStr	Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method
title_full_unstemmed	Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method
title_sort	optical properties of fe2+ ion doped zns nanoparticles synthesized using co-precipitation method
publisher	Fakulti Kejuruteraan ,UKM,Bangi.
publishDate	2015
url	http://journalarticle.ukm.my/9512/ http://journalarticle.ukm.my/9512/ http://journalarticle.ukm.my/9512/1/12.pdf
first_indexed	2023-09-18T19:55:05Z
last_indexed	2023-09-18T19:55:05Z
_version_	1777406475478499328

Optical properties of Fe2+ Ion doped ZnS nanoparticles synthesized using co-precipitation method

Similar Items