Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method

Efforts were given to find suitable method to produce hard and coherent water adsorbent for ethanol water mixture. Three methods were studied. In the first method, calcined clay was mixed with alumina and KOH or NaOH. Water was added to get 40-50% solution and thoroughly...

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Main Authors: A .A., Azharin Shah, Nour, A. H., R. M., Yunus
Format: Article
Language:English
English
Published: AENSI Publishing 2014
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/12587/
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http://umpir.ump.edu.my/id/eprint/12587/1/fkksa-2014-abrahman-Methodology%20To%20Produce%20Hard%20Coherent%20Water%20Adsorbent%20Using%20Modified%20Fusion.pdf
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spelling ump-125872018-01-15T03:40:01Z http://umpir.ump.edu.my/id/eprint/12587/ Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method A .A., Azharin Shah Nour, A. H. R. M., Yunus TP Chemical technology Efforts were given to find suitable method to produce hard and coherent water adsorbent for ethanol water mixture. Three methods were studied. In the first method, calcined clay was mixed with alumina and KOH or NaOH. Water was added to get 40-50% solution and thoroughly mixed. The mixture was aged for 48 hours in closed container at 38oC followed by crystallization. In the second method, calcined clay or pure silica and alumina sources were mixed with NaOH or KOH and fused in furnace at 550oC for 12 hours. The fused mixture was mixed with water to get 40-55% solution of KOH or NaOH. Aging was carried out at 38oC for 48 hours before crystallization took place. In the third method, fused mixture from method 2 was mixed with NaOH or KOH and 5 part of water. The mixture was vigorously stirred for 3 hours and left for aging/crystallization at 60oC for 24 hours in oven. All the products from the three methodologies were washed and dried before being tested for water adsorbance. Results showed that method 2 was able to produce water adsorbent. The experimental results also revealed that the repetition of reflux may improve the water adsorbance performance of the adsorbent. However XRD analysis showed that the product was not the type of zeolite A. AENSI Publishing 2014 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/12587/1/fkksa-2014-abrahman-Methodology%20To%20Produce%20Hard%20Coherent%20Water%20Adsorbent%20Using%20Modified%20Fusion.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/12587/7/fkksa-2014-abrahman-Methodology%20To%20Produce%20Hard%20Coherent%20Water%20Adsorbent%20Using%20Modified%20Fusion.pdf A .A., Azharin Shah and Nour, A. H. and R. M., Yunus (2014) Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method. Australian Journal of Basic and Applied Sciences, 8 (4). pp. 235-240. ISSN 1991-8178 http://www.ajbasweb.com/old/ajbas/2014/Special/235-240.pdf
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
topic TP Chemical technology
spellingShingle TP Chemical technology
A .A., Azharin Shah
Nour, A. H.
R. M., Yunus
Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method
description Efforts were given to find suitable method to produce hard and coherent water adsorbent for ethanol water mixture. Three methods were studied. In the first method, calcined clay was mixed with alumina and KOH or NaOH. Water was added to get 40-50% solution and thoroughly mixed. The mixture was aged for 48 hours in closed container at 38oC followed by crystallization. In the second method, calcined clay or pure silica and alumina sources were mixed with NaOH or KOH and fused in furnace at 550oC for 12 hours. The fused mixture was mixed with water to get 40-55% solution of KOH or NaOH. Aging was carried out at 38oC for 48 hours before crystallization took place. In the third method, fused mixture from method 2 was mixed with NaOH or KOH and 5 part of water. The mixture was vigorously stirred for 3 hours and left for aging/crystallization at 60oC for 24 hours in oven. All the products from the three methodologies were washed and dried before being tested for water adsorbance. Results showed that method 2 was able to produce water adsorbent. The experimental results also revealed that the repetition of reflux may improve the water adsorbance performance of the adsorbent. However XRD analysis showed that the product was not the type of zeolite A.
format Article
author A .A., Azharin Shah
Nour, A. H.
R. M., Yunus
author_facet A .A., Azharin Shah
Nour, A. H.
R. M., Yunus
author_sort A .A., Azharin Shah
title Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method
title_short Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method
title_full Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method
title_fullStr Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method
title_full_unstemmed Methodology to Produce Hard Coherent Water Adsorbent Using Modified Fusion Method
title_sort methodology to produce hard coherent water adsorbent using modified fusion method
publisher AENSI Publishing
publishDate 2014
url http://umpir.ump.edu.my/id/eprint/12587/
http://umpir.ump.edu.my/id/eprint/12587/
http://umpir.ump.edu.my/id/eprint/12587/1/fkksa-2014-abrahman-Methodology%20To%20Produce%20Hard%20Coherent%20Water%20Adsorbent%20Using%20Modified%20Fusion.pdf
http://umpir.ump.edu.my/id/eprint/12587/7/fkksa-2014-abrahman-Methodology%20To%20Produce%20Hard%20Coherent%20Water%20Adsorbent%20Using%20Modified%20Fusion.pdf
first_indexed 2023-09-18T22:14:23Z
last_indexed 2023-09-18T22:14:23Z
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