Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle

Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle

In this study, sol–gel technique has been used to prepare nanoparticle Mg doped ZnO with 2 wt. % at low pH without using any capping or surfactant agent. The Mg-ZnO nanostructure, surface area and porosity, surface morphology and element analysis was analyzed by X-Ray Diffraction (XRD), Fourier Tran...

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Main Authors: Wafaa, A. Khadim, Mohd Hasbi, Ab. Rahim
Format: Conference or Workshop Item
Language:English
English
Published: EDP Sciences 2017
Subjects:
Q Science (General)
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/18107/
http://umpir.ump.edu.my/id/eprint/18107/
http://umpir.ump.edu.my/id/eprint/18107/1/Surfactant-less%20Sol-Gel%20Technique%20for%20the%20Synthesis%20of%20Mg-ZnO%20Nanoparticle.pdf
http://umpir.ump.edu.my/id/eprint/18107/7/Surfactant-less%20Sol-Gel%20Technique%20for%20the%20Synthesis%20of%20Mg-ZnO%20Nanoparticle%201.pdf
id ump-18107
recordtype eprints
spelling ump-181072018-11-22T06:42:17Z http://umpir.ump.edu.my/id/eprint/18107/ Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle Wafaa, A. Khadim Mohd Hasbi, Ab. Rahim Q Science (General) TP Chemical technology In this study, sol–gel technique has been used to prepare nanoparticle Mg doped ZnO with 2 wt. % at low pH without using any capping or surfactant agent. The Mg-ZnO nanostructure, surface area and porosity, surface morphology and element analysis was analyzed by X-Ray Diffraction (XRD), Fourier Transforms Infra-Red (FTIR), N2 Physisorption and Field Emission Scanning Electron Microscopy with energy dispersive X-ray spectroscopy (FESEM-EDX). The characterizations confirmed that the surfactant is not necessary for sol-gel synthesis technique, whereby highly crystalline material with smaller crystallite size (30nm) and high surface area (21.7) was obtained. Besides, the synthesis approach is useful for accurately immobilized the required amount of Mg as doping element on ZnO material with the accuracy up to 99.5% confirmed through EDX analysis. EDP Sciences 2017 Conference or Workshop Item PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/18107/1/Surfactant-less%20Sol-Gel%20Technique%20for%20the%20Synthesis%20of%20Mg-ZnO%20Nanoparticle.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/18107/7/Surfactant-less%20Sol-Gel%20Technique%20for%20the%20Synthesis%20of%20Mg-ZnO%20Nanoparticle%201.pdf Wafaa, A. Khadim and Mohd Hasbi, Ab. Rahim (2017) Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle. In: INTERNATIONAL CONFERENCE ON FLUIDS & CHEMICAL ENGINEERING 2017, 4-6 April 2017 , Sabah, Malaysia. pp. 1-4., 111. ISSN 2261-236X https://www.matec-conferences.org/articles/matecconf/abs/2017/25/matecconf_fluid2017_02006/matecconf_fluid2017_02006.html
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
topic Q Science (General)
TP Chemical technology
spellingShingle Q Science (General)
TP Chemical technology
Wafaa, A. Khadim
Mohd Hasbi, Ab. Rahim
Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle
description In this study, sol–gel technique has been used to prepare nanoparticle Mg doped ZnO with 2 wt. % at low pH without using any capping or surfactant agent. The Mg-ZnO nanostructure, surface area and porosity, surface morphology and element analysis was analyzed by X-Ray Diffraction (XRD), Fourier Transforms Infra-Red (FTIR), N2 Physisorption and Field Emission Scanning Electron Microscopy with energy dispersive X-ray spectroscopy (FESEM-EDX). The characterizations confirmed that the surfactant is not necessary for sol-gel synthesis technique, whereby highly crystalline material with smaller crystallite size (30nm) and high surface area (21.7) was obtained. Besides, the synthesis approach is useful for accurately immobilized the required amount of Mg as doping element on ZnO material with the accuracy up to 99.5% confirmed through EDX analysis.
format Conference or Workshop Item
author Wafaa, A. Khadim
Mohd Hasbi, Ab. Rahim
author_facet Wafaa, A. Khadim
Mohd Hasbi, Ab. Rahim
author_sort Wafaa, A. Khadim
title Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle
title_short Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle
title_full Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle
title_fullStr Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle
title_full_unstemmed Surfactant-less Sol-Gel Technique for the Synthesis of Mg-ZnO Nanoparticle
title_sort surfactant-less sol-gel technique for the synthesis of mg-zno nanoparticle
publisher EDP Sciences
publishDate 2017
url http://umpir.ump.edu.my/id/eprint/18107/
http://umpir.ump.edu.my/id/eprint/18107/
http://umpir.ump.edu.my/id/eprint/18107/1/Surfactant-less%20Sol-Gel%20Technique%20for%20the%20Synthesis%20of%20Mg-ZnO%20Nanoparticle.pdf
http://umpir.ump.edu.my/id/eprint/18107/7/Surfactant-less%20Sol-Gel%20Technique%20for%20the%20Synthesis%20of%20Mg-ZnO%20Nanoparticle%201.pdf
first_indexed 2023-09-18T22:25:27Z
last_indexed 2023-09-18T22:25:27Z
_version_ 1777415935827640320

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