Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium

Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium

Unique optical and physical behaviour of nanoparticles compared to corresponding bulk materials has gain considerably interest and the research in synthesizing and application of nanoparticles has expanded rapidly over a last decade. This present study reported on the well-dispersity synthesis of na...

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Main Authors: Nurul Akma, Reduan, Suriati, Ghazali, Saidatul Shima, Jamari
Format: Article
Language:English
English
Published: Asian Research Publishing Network (ARPN) 2016
Subjects:
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/18482/
http://umpir.ump.edu.my/id/eprint/18482/
http://umpir.ump.edu.my/id/eprint/18482/1/Effect%20Of%20Temperature%20And%20NaCl%20Concentration%20On%20Synthesis%20Of%20Silver%20Nanoparticles%20Prepared%20In%20Aqueous%20Medium.pdf
http://umpir.ump.edu.my/id/eprint/18482/2/Effect%20Of%20Temperature%20And%20NaCl%20Concentration%20On%20Synthesis%20Of%20Silver%20Nanoparticles%20Prepared%20In%20Aqueous%20Medium%201.pdf
id ump-18482
recordtype eprints
spelling ump-184822019-10-30T07:30:32Z http://umpir.ump.edu.my/id/eprint/18482/ Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium Nurul Akma, Reduan Suriati, Ghazali Saidatul Shima, Jamari TP Chemical technology Unique optical and physical behaviour of nanoparticles compared to corresponding bulk materials has gain considerably interest and the research in synthesizing and application of nanoparticles has expanded rapidly over a last decade. This present study reported on the well-dispersity synthesis of nano-size material via chemical reduction of silver nitrate (AgNO3) by sodium borohydride (NaBH4) in an aqueous medium. In this study, there are two parameters that were manipulated which are temperatures; varied from 25 °C until 90 °C and concentration of sodium chloride (NaCl) that was varied from 0.0mM to 30.0 mM respectively. The UV-Vis analysis of silver nanoparticles shows maximum peak were determined at the range of 404nm- 410 nm which is the characteristic of Ag particles. Meanwhile, the morphology of assynthesized silver nanoparticles (AgNPs) that investigated by using Field Emission Scanning Electron Microscopy (FESEM) reveals a spherical particles size with the size range of 20 nm-160 nm. Analysis of AgNPs diameter by using Image J reveal that the smallest nano-size AgNPs is at 3.0 mM NaCl and at temperature 45°C which is ~50 nm. Asian Research Publishing Network (ARPN) 2016 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/18482/1/Effect%20Of%20Temperature%20And%20NaCl%20Concentration%20On%20Synthesis%20Of%20Silver%20Nanoparticles%20Prepared%20In%20Aqueous%20Medium.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/18482/2/Effect%20Of%20Temperature%20And%20NaCl%20Concentration%20On%20Synthesis%20Of%20Silver%20Nanoparticles%20Prepared%20In%20Aqueous%20Medium%201.pdf Nurul Akma, Reduan and Suriati, Ghazali and Saidatul Shima, Jamari (2016) Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium. ARPN Journal of Engineering and Applied Sciences, 11 (10). pp. 6399-6404. ISSN 1819-6608 http://www.arpnjournals.org/jeas/research_papers/rp_2016/jeas_0516_4287.pdf
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
topic TP Chemical technology
spellingShingle TP Chemical technology
Nurul Akma, Reduan
Suriati, Ghazali
Saidatul Shima, Jamari
Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium
description Unique optical and physical behaviour of nanoparticles compared to corresponding bulk materials has gain considerably interest and the research in synthesizing and application of nanoparticles has expanded rapidly over a last decade. This present study reported on the well-dispersity synthesis of nano-size material via chemical reduction of silver nitrate (AgNO3) by sodium borohydride (NaBH4) in an aqueous medium. In this study, there are two parameters that were manipulated which are temperatures; varied from 25 °C until 90 °C and concentration of sodium chloride (NaCl) that was varied from 0.0mM to 30.0 mM respectively. The UV-Vis analysis of silver nanoparticles shows maximum peak were determined at the range of 404nm- 410 nm which is the characteristic of Ag particles. Meanwhile, the morphology of assynthesized silver nanoparticles (AgNPs) that investigated by using Field Emission Scanning Electron Microscopy (FESEM) reveals a spherical particles size with the size range of 20 nm-160 nm. Analysis of AgNPs diameter by using Image J reveal that the smallest nano-size AgNPs is at 3.0 mM NaCl and at temperature 45°C which is ~50 nm.
format Article
author Nurul Akma, Reduan
Suriati, Ghazali
Saidatul Shima, Jamari
author_facet Nurul Akma, Reduan
Suriati, Ghazali
Saidatul Shima, Jamari
author_sort Nurul Akma, Reduan
title Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium
title_short Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium
title_full Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium
title_fullStr Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium
title_full_unstemmed Effect Of Temperature And NaCl Concentration On Synthesis Of Silver Nanoparticles Prepared In Aqueous Medium
title_sort effect of temperature and nacl concentration on synthesis of silver nanoparticles prepared in aqueous medium
publisher Asian Research Publishing Network (ARPN)
publishDate 2016
url http://umpir.ump.edu.my/id/eprint/18482/
http://umpir.ump.edu.my/id/eprint/18482/
http://umpir.ump.edu.my/id/eprint/18482/1/Effect%20Of%20Temperature%20And%20NaCl%20Concentration%20On%20Synthesis%20Of%20Silver%20Nanoparticles%20Prepared%20In%20Aqueous%20Medium.pdf
http://umpir.ump.edu.my/id/eprint/18482/2/Effect%20Of%20Temperature%20And%20NaCl%20Concentration%20On%20Synthesis%20Of%20Silver%20Nanoparticles%20Prepared%20In%20Aqueous%20Medium%201.pdf
first_indexed 2023-09-18T22:26:12Z
last_indexed 2023-09-18T22:26:12Z
_version_ 1777415983164555264

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