Carbon quantum dots assisted graphene exfoliation derived activated carbon

Graphene is deemed as the strongest and toughest material since its discovery in 2004 by Andre Geim and Konstantin Novoselov as it offers exceptional potential in electronic, thermal and mechanical properties for various application in future. Graphene can be derived from any materials that have pre...

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Main Author: Norshahirah Nadiah, Abd Rahman
Format: Undergraduates Project Papers
Language:English
English
English
English
Published: 2016
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/19281/
http://umpir.ump.edu.my/id/eprint/19281/
http://umpir.ump.edu.my/id/eprint/19281/1/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Table%20of%20contents.pdf
http://umpir.ump.edu.my/id/eprint/19281/2/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Abstract.pdf
http://umpir.ump.edu.my/id/eprint/19281/3/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Chapter%201.pdf
http://umpir.ump.edu.my/id/eprint/19281/4/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-References.pdf
id ump-19281
recordtype eprints
spelling ump-192812017-12-19T03:35:12Z http://umpir.ump.edu.my/id/eprint/19281/ Carbon quantum dots assisted graphene exfoliation derived activated carbon Norshahirah Nadiah, Abd Rahman TA Engineering (General). Civil engineering (General) Graphene is deemed as the strongest and toughest material since its discovery in 2004 by Andre Geim and Konstantin Novoselov as it offers exceptional potential in electronic, thermal and mechanical properties for various application in future. Graphene can be derived from any materials that have presence of carbon in its structure and can be exfoliated in various ways including wet chemicals route. However, chemical reduction of graphene from any carbon sources is highly toxic and harmful to human‟s health and environment. In this study, an environmental friendly approach to exfoliate graphene is proposed where graphene is derived from activated carbon (AC) and water as solvent through liquid phase exfoliation method. The exfoliation is assisted by sonication process where the induced microbubbles due to cavitation will collapse and release a tremendous amount of energy to exfoliate graphene from AC. Since water has high surface tension, carbon quantum dots (CQDs) is added to reduce the surface tension to the optimum range and as an exfoliation agent. The CQDs is synthesized from citric acid and urea by microwave irradiation. Dialysis process of CQDs solution is done to remove large and unreacted particles to obtained fine particle size of CQDs. The morphology of exfoliated graphene and CQDs is confirmed by FESEM analysis. The functional groups for exfoliated graphene and CQDs are determined by FT-IR (ATR) spectroscopy analysis. The concentration of exfoliated graphene obtained is calculated by linear regression equation obtained from a standard curve of graphene where 0.01177 mg/mL is produced from 24 mg of activated carbon. 2016-12 Undergraduates Project Papers NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/19281/1/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Table%20of%20contents.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/19281/2/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Abstract.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/19281/3/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Chapter%201.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/19281/4/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-References.pdf Norshahirah Nadiah, Abd Rahman (2016) Carbon quantum dots assisted graphene exfoliation derived activated carbon. Faculty of Industrial Sciences and Technology, Universiti Malaysia Pahang. http://iportal.ump.edu.my/lib/item?id=chamo:102316&theme=UMP2
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
English
English
English
topic TA Engineering (General). Civil engineering (General)
spellingShingle TA Engineering (General). Civil engineering (General)
Norshahirah Nadiah, Abd Rahman
Carbon quantum dots assisted graphene exfoliation derived activated carbon
description Graphene is deemed as the strongest and toughest material since its discovery in 2004 by Andre Geim and Konstantin Novoselov as it offers exceptional potential in electronic, thermal and mechanical properties for various application in future. Graphene can be derived from any materials that have presence of carbon in its structure and can be exfoliated in various ways including wet chemicals route. However, chemical reduction of graphene from any carbon sources is highly toxic and harmful to human‟s health and environment. In this study, an environmental friendly approach to exfoliate graphene is proposed where graphene is derived from activated carbon (AC) and water as solvent through liquid phase exfoliation method. The exfoliation is assisted by sonication process where the induced microbubbles due to cavitation will collapse and release a tremendous amount of energy to exfoliate graphene from AC. Since water has high surface tension, carbon quantum dots (CQDs) is added to reduce the surface tension to the optimum range and as an exfoliation agent. The CQDs is synthesized from citric acid and urea by microwave irradiation. Dialysis process of CQDs solution is done to remove large and unreacted particles to obtained fine particle size of CQDs. The morphology of exfoliated graphene and CQDs is confirmed by FESEM analysis. The functional groups for exfoliated graphene and CQDs are determined by FT-IR (ATR) spectroscopy analysis. The concentration of exfoliated graphene obtained is calculated by linear regression equation obtained from a standard curve of graphene where 0.01177 mg/mL is produced from 24 mg of activated carbon.
format Undergraduates Project Papers
author Norshahirah Nadiah, Abd Rahman
author_facet Norshahirah Nadiah, Abd Rahman
author_sort Norshahirah Nadiah, Abd Rahman
title Carbon quantum dots assisted graphene exfoliation derived activated carbon
title_short Carbon quantum dots assisted graphene exfoliation derived activated carbon
title_full Carbon quantum dots assisted graphene exfoliation derived activated carbon
title_fullStr Carbon quantum dots assisted graphene exfoliation derived activated carbon
title_full_unstemmed Carbon quantum dots assisted graphene exfoliation derived activated carbon
title_sort carbon quantum dots assisted graphene exfoliation derived activated carbon
publishDate 2016
url http://umpir.ump.edu.my/id/eprint/19281/
http://umpir.ump.edu.my/id/eprint/19281/
http://umpir.ump.edu.my/id/eprint/19281/1/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Table%20of%20contents.pdf
http://umpir.ump.edu.my/id/eprint/19281/2/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Abstract.pdf
http://umpir.ump.edu.my/id/eprint/19281/3/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-Chapter%201.pdf
http://umpir.ump.edu.my/id/eprint/19281/4/Carbon%20quantum%20dots%20assisted%20graphene%20exfoliation%20derived%20activated%20carbon%20-References.pdf
first_indexed 2023-09-18T22:27:39Z
last_indexed 2023-09-18T22:27:39Z
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