Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power

Mace essential oil extractions were carried out using hydrodistillation (HD) and microwave assisted hydrodistillation (MAHD). The powers used were varied from 300, 600, and 800 W. The amounts of oil from dew resulted from condensation were measured every 1 min. The condensation was done using 12 °C...

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Main Authors: Megawati, ., Fardhyanti, Dewi Selvia, Sediawan, Wahyudi Budi, Anwaruddin, Hisyam
Format: Article
Language:English
Published: Elsevier Ltd 2019
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Online Access:http://umpir.ump.edu.my/id/eprint/24242/
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http://umpir.ump.edu.my/id/eprint/24242/1/Kinetics%20of%20mace%20%28Myristicae%20arillus%29%20essential%20oil%20extraction%20using%20microwave%20assisted%20hydrodistillation.pdf
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spelling ump-242422019-03-19T03:31:10Z http://umpir.ump.edu.my/id/eprint/24242/ Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power Megawati, . Fardhyanti, Dewi Selvia Sediawan, Wahyudi Budi Anwaruddin, Hisyam TP Chemical technology Mace essential oil extractions were carried out using hydrodistillation (HD) and microwave assisted hydrodistillation (MAHD). The powers used were varied from 300, 600, and 800 W. The amounts of oil from dew resulted from condensation were measured every 1 min. The condensation was done using 12 °C cold water. From the experimental results, MAHD is seen to be superior to HD. The extraction using MAHD at 800 W stopped after 20 min (8.63% yield), while the one using HD stopped after 73 min (7.03% yield). The power used affected the yields of essential oils obtained. From the various powers used, in 10 min, the yields obtained were 2.68, 4.56, 5.41%, in 15 min 4.12, 6.20, 6.83%, and in 20 min 5.13, 7.39, 6.83% at 300, 600, and 800 W, respectively. It can also be seen that time has a significant effect on the essential oil yields obtained. The main components of the essential oil obtained from HD and MAHD were beta pinene, alpha pinene, myristicin, 4-terpineol, and gamma terpinene. The mechanism of mace essential oil mass transfer using HD and MAHD methods was controlled by intra-particle diffusion following the Fick’s law. The diffusion coefficient (De) of HD was 4.98 × 10−14 m2/s and the diffusion coefficients of MAHD were 9.17 × 10−14, 1.39 × 10−13, and 1.65 × 10−13 m2/s at 300, 600, and 800 W, respectively. The empirical correlation of diffusion coefficient and MAHD power can be approximated by De = 3.02 × 10−15 × P0.5985. Elsevier Ltd 2019 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/24242/1/Kinetics%20of%20mace%20%28Myristicae%20arillus%29%20essential%20oil%20extraction%20using%20microwave%20assisted%20hydrodistillation.pdf Megawati, . and Fardhyanti, Dewi Selvia and Sediawan, Wahyudi Budi and Anwaruddin, Hisyam (2019) Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power. Industrial Crops and Products, 131. pp. 315-322. ISSN 0926-6690 https://doi.org/10.1016/j.indcrop.2019.01.067 https://doi.org/10.1016/j.indcrop.2019.01.067
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Megawati, .
Fardhyanti, Dewi Selvia
Sediawan, Wahyudi Budi
Anwaruddin, Hisyam
Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power
description Mace essential oil extractions were carried out using hydrodistillation (HD) and microwave assisted hydrodistillation (MAHD). The powers used were varied from 300, 600, and 800 W. The amounts of oil from dew resulted from condensation were measured every 1 min. The condensation was done using 12 °C cold water. From the experimental results, MAHD is seen to be superior to HD. The extraction using MAHD at 800 W stopped after 20 min (8.63% yield), while the one using HD stopped after 73 min (7.03% yield). The power used affected the yields of essential oils obtained. From the various powers used, in 10 min, the yields obtained were 2.68, 4.56, 5.41%, in 15 min 4.12, 6.20, 6.83%, and in 20 min 5.13, 7.39, 6.83% at 300, 600, and 800 W, respectively. It can also be seen that time has a significant effect on the essential oil yields obtained. The main components of the essential oil obtained from HD and MAHD were beta pinene, alpha pinene, myristicin, 4-terpineol, and gamma terpinene. The mechanism of mace essential oil mass transfer using HD and MAHD methods was controlled by intra-particle diffusion following the Fick’s law. The diffusion coefficient (De) of HD was 4.98 × 10−14 m2/s and the diffusion coefficients of MAHD were 9.17 × 10−14, 1.39 × 10−13, and 1.65 × 10−13 m2/s at 300, 600, and 800 W, respectively. The empirical correlation of diffusion coefficient and MAHD power can be approximated by De = 3.02 × 10−15 × P0.5985.
format Article
author Megawati, .
Fardhyanti, Dewi Selvia
Sediawan, Wahyudi Budi
Anwaruddin, Hisyam
author_facet Megawati, .
Fardhyanti, Dewi Selvia
Sediawan, Wahyudi Budi
Anwaruddin, Hisyam
author_sort Megawati, .
title Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power
title_short Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power
title_full Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power
title_fullStr Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power
title_full_unstemmed Kinetics of mace (Myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: Effect of microwave power
title_sort kinetics of mace (myristicae arillus) essential oil extraction using microwave assisted hydrodistillation: effect of microwave power
publisher Elsevier Ltd
publishDate 2019
url http://umpir.ump.edu.my/id/eprint/24242/
http://umpir.ump.edu.my/id/eprint/24242/
http://umpir.ump.edu.my/id/eprint/24242/
http://umpir.ump.edu.my/id/eprint/24242/1/Kinetics%20of%20mace%20%28Myristicae%20arillus%29%20essential%20oil%20extraction%20using%20microwave%20assisted%20hydrodistillation.pdf
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