Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane

Supported liquid membrane (SLM) is the most effective technique to extract and recover the desired product from the biomass products in a single step. The study of the operation parameters in SLM system is very important to improve the yield of extraction and recovery of the product. In this study,...

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Main Authors: Rajendran, V., Syed Mohd Saufi, Tuan Chik, Mior Ahmad Khushairi, Mohd Zahari, Mohammad, A. W.
Format: Article
Language:English
Published: Penerbit UMP 2019
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/26058/
http://umpir.ump.edu.my/id/eprint/26058/
http://umpir.ump.edu.my/id/eprint/26058/
http://umpir.ump.edu.my/id/eprint/26058/1/Study%20on%20stripping%20phase%20conditions%20on%20the%20levulinic.pdf
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spelling ump-260582019-11-21T04:30:15Z http://umpir.ump.edu.my/id/eprint/26058/ Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane Rajendran, V. Syed Mohd Saufi, Tuan Chik Mior Ahmad Khushairi, Mohd Zahari Mohammad, A. W. QD Chemistry TP Chemical technology Supported liquid membrane (SLM) is the most effective technique to extract and recover the desired product from the biomass products in a single step. The study of the operation parameters in SLM system is very important to improve the yield of extraction and recovery of the product. In this study, different types of stripping agents such as sodium hydroxide (NaOH), sodium carbonate, hydrochloric acid, trimethylamine, and water were tested in the SLM system to extract levulinic acid (LA). By using 0.3 M trioctylamine in 2-ethyl-1-hexanol as liquid membrane phase, it was found that NaOH was the best stripping agent to extract LA. The concentration of the NaOH stripping agent was varied from 0.25 M to 1 M. The best stripping agent concentration was 0.5 M, which gave an LA extraction of 86% from a 10 g/L LA aqueous solution. The flow rate of the feed and stripping phase was investigated from 25 mL/min to 125 mL/min. SLM operated at 75 L/min was found to be adequate in reducing the boundary layer thickness at both sides of the SLM phases without any leakage of the liquid membrane and breakage of the matrix support. At the best stripping condition, 89% of the LA was extracted using 0.5 M NaOH that operated at flow rate of 75 mL/min. Penerbit UMP 2019-09-27 Article PeerReviewed pdf en cc_by_nc_4 http://umpir.ump.edu.my/id/eprint/26058/1/Study%20on%20stripping%20phase%20conditions%20on%20the%20levulinic.pdf Rajendran, V. and Syed Mohd Saufi, Tuan Chik and Mior Ahmad Khushairi, Mohd Zahari and Mohammad, A. W. (2019) Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane. Journal of Mechanical Engineering and Sciences (JMES), 13 (3). 5625 -5636. ISSN 2289-4659 (print); 2231-8380 (online) http://journal.ump.edu.my/jmes/article/view/1702 https://doi.org/10.15282/jmes.13.3.2019.25.0451
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic QD Chemistry
TP Chemical technology
spellingShingle QD Chemistry
TP Chemical technology
Rajendran, V.
Syed Mohd Saufi, Tuan Chik
Mior Ahmad Khushairi, Mohd Zahari
Mohammad, A. W.
Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane
description Supported liquid membrane (SLM) is the most effective technique to extract and recover the desired product from the biomass products in a single step. The study of the operation parameters in SLM system is very important to improve the yield of extraction and recovery of the product. In this study, different types of stripping agents such as sodium hydroxide (NaOH), sodium carbonate, hydrochloric acid, trimethylamine, and water were tested in the SLM system to extract levulinic acid (LA). By using 0.3 M trioctylamine in 2-ethyl-1-hexanol as liquid membrane phase, it was found that NaOH was the best stripping agent to extract LA. The concentration of the NaOH stripping agent was varied from 0.25 M to 1 M. The best stripping agent concentration was 0.5 M, which gave an LA extraction of 86% from a 10 g/L LA aqueous solution. The flow rate of the feed and stripping phase was investigated from 25 mL/min to 125 mL/min. SLM operated at 75 L/min was found to be adequate in reducing the boundary layer thickness at both sides of the SLM phases without any leakage of the liquid membrane and breakage of the matrix support. At the best stripping condition, 89% of the LA was extracted using 0.5 M NaOH that operated at flow rate of 75 mL/min.
format Article
author Rajendran, V.
Syed Mohd Saufi, Tuan Chik
Mior Ahmad Khushairi, Mohd Zahari
Mohammad, A. W.
author_facet Rajendran, V.
Syed Mohd Saufi, Tuan Chik
Mior Ahmad Khushairi, Mohd Zahari
Mohammad, A. W.
author_sort Rajendran, V.
title Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane
title_short Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane
title_full Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane
title_fullStr Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane
title_full_unstemmed Study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane
title_sort study on stripping phase conditions on the levulinic acid extraction using supported liquid membrane
publisher Penerbit UMP
publishDate 2019
url http://umpir.ump.edu.my/id/eprint/26058/
http://umpir.ump.edu.my/id/eprint/26058/
http://umpir.ump.edu.my/id/eprint/26058/
http://umpir.ump.edu.my/id/eprint/26058/1/Study%20on%20stripping%20phase%20conditions%20on%20the%20levulinic.pdf
first_indexed 2023-09-18T22:40:20Z
last_indexed 2023-09-18T22:40:20Z
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