Batch solvent extraction of caffeine from MCBC2

Caffeine is a naturally occurring substance found in cocoa seeds. The aim of this research is to extract caffeine from Malaysian Cocoa Board Clone (MCBC) 2, and to investigate the effect of sample particle size, solvent/feed ratio, and extraction time on the yield of caffeine. The sample was prepare...

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Main Author: Nedunjeliyan, Dinesh Varma
Format: Undergraduates Project Papers
Language:English
Published: 2010
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/3317/
http://umpir.ump.edu.my/id/eprint/3317/
http://umpir.ump.edu.my/id/eprint/3317/1/CD5520_DINESH_VARMA_AL_NEDUNJELIYAN.pdf
id ump-3317
recordtype eprints
spelling ump-33172015-03-03T08:00:30Z http://umpir.ump.edu.my/id/eprint/3317/ Batch solvent extraction of caffeine from MCBC2 Nedunjeliyan, Dinesh Varma TP Chemical technology Caffeine is a naturally occurring substance found in cocoa seeds. The aim of this research is to extract caffeine from Malaysian Cocoa Board Clone (MCBC) 2, and to investigate the effect of sample particle size, solvent/feed ratio, and extraction time on the yield of caffeine. The sample was prepared by grinding and sieving, followed by solid-liquid extraction using water by heat reflux extracting technique, liquid-liquid extraction with ethyl acetate, drying of caffeine by rotary evaporator, and finally analysis of the caffeine yield. The analysis of the caffeine yield was done using UV/Vis Spectrophotometric method. The caffeine yield was highest at sample particle size of 400µm (0.35 % w/w caffeine or 3.4956 mg/g cocoa), solvent/feed ratio of 1:1 (0.35 % w/w caffeine or 3.5066 mg/g cocoa), and extraction time of 90 minutes (0.34 % w/w caffeine or 3.4356 mg/g cocoa). The best conditions for the highest yield of caffeine from MCBC2 were 400µm of sample particle size, 1:1 of solvent/feed ratio, and 90 minutes of extraction time. 2010-09 Undergraduates Project Papers NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/3317/1/CD5520_DINESH_VARMA_AL_NEDUNJELIYAN.pdf Nedunjeliyan, Dinesh Varma (2010) Batch solvent extraction of caffeine from MCBC2. Faculty of Chemical and Natural Resources Engineering , Universiti Malaysia Pahang . http://iportal.ump.edu.my/lib/item?id=chamo:56241&theme=UMP2
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Nedunjeliyan, Dinesh Varma
Batch solvent extraction of caffeine from MCBC2
description Caffeine is a naturally occurring substance found in cocoa seeds. The aim of this research is to extract caffeine from Malaysian Cocoa Board Clone (MCBC) 2, and to investigate the effect of sample particle size, solvent/feed ratio, and extraction time on the yield of caffeine. The sample was prepared by grinding and sieving, followed by solid-liquid extraction using water by heat reflux extracting technique, liquid-liquid extraction with ethyl acetate, drying of caffeine by rotary evaporator, and finally analysis of the caffeine yield. The analysis of the caffeine yield was done using UV/Vis Spectrophotometric method. The caffeine yield was highest at sample particle size of 400µm (0.35 % w/w caffeine or 3.4956 mg/g cocoa), solvent/feed ratio of 1:1 (0.35 % w/w caffeine or 3.5066 mg/g cocoa), and extraction time of 90 minutes (0.34 % w/w caffeine or 3.4356 mg/g cocoa). The best conditions for the highest yield of caffeine from MCBC2 were 400µm of sample particle size, 1:1 of solvent/feed ratio, and 90 minutes of extraction time.
format Undergraduates Project Papers
author Nedunjeliyan, Dinesh Varma
author_facet Nedunjeliyan, Dinesh Varma
author_sort Nedunjeliyan, Dinesh Varma
title Batch solvent extraction of caffeine from MCBC2
title_short Batch solvent extraction of caffeine from MCBC2
title_full Batch solvent extraction of caffeine from MCBC2
title_fullStr Batch solvent extraction of caffeine from MCBC2
title_full_unstemmed Batch solvent extraction of caffeine from MCBC2
title_sort batch solvent extraction of caffeine from mcbc2
publishDate 2010
url http://umpir.ump.edu.my/id/eprint/3317/
http://umpir.ump.edu.my/id/eprint/3317/
http://umpir.ump.edu.my/id/eprint/3317/1/CD5520_DINESH_VARMA_AL_NEDUNJELIYAN.pdf
first_indexed 2023-09-18T21:57:31Z
last_indexed 2023-09-18T21:57:31Z
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