Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide
The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in w...
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| Format: | Article |
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Springer
1997
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| Online Access: | http://umpir.ump.edu.my/id/eprint/4772/ http://umpir.ump.edu.my/id/eprint/4772/ http://umpir.ump.edu.my/id/eprint/4772/ |
| Summary: | The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in with four molecules per unit cell. Crystal Data: a - 10.483(2) A, h - 6.206(I) A, c = 24.767(5) A, [3 - 90.39(3), V = 1611.5(6) A ~, R(F)[I > 2r = 0.0679, wR(F 2) [1 > 2or(l)] = 0. 1148.
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