Synthesis, characterization and catalytic activity of Ni supported on bleaching clay

Bleaching clay samples from Hudson WA Sdn Bhd were used to synthesis Ni(II) supported on clay. Metal supported on clay can serve as catalyst for hydrogenation reaction of crude palm oil. Acid analyses were employed using Ion Chromatography and titration technique to determine type and acid content....

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Main Author:	Mohd Alias, Ahmad
Format:	Undergraduates Project Papers
Language:	English
Published:	2012
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/7797/ http://umpir.ump.edu.my/id/eprint/7797/ http://umpir.ump.edu.my/id/eprint/7797/1/MOHD_ALIAS_BIN_AHMAD.PDF

id	ump-7797
recordtype	eprints
spelling	ump-77972016-06-24T07:34:03Z http://umpir.ump.edu.my/id/eprint/7797/ Synthesis, characterization and catalytic activity of Ni supported on bleaching clay Mohd Alias, Ahmad TP Chemical technology Bleaching clay samples from Hudson WA Sdn Bhd were used to synthesis Ni(II) supported on clay. Metal supported on clay can serve as catalyst for hydrogenation reaction of crude palm oil. Acid analyses were employed using Ion Chromatography and titration technique to determine type and acid content. The nature of the bleaching clay examined by using X-ray Diffraction (XRI)), Thermal Gravimetric Analysis (TGA), Fourier Transform Infrared (FTIR) and BET surface area. Nickel acetate with ethylene glycol as reducing agent was treated with bleaching clay to absorp metal: onto and into the interlayer of the clay. The adsorption of Ni(II) was investigated using BET surface area and x-ray diffraction. IC analysis and acid-base titration showed acid sulphuric as dominant acid at 0.0615 wt %. FTIR spectra and XRD pattern of this clay is identical with jute mineral It has a lattice spacing of 10.67 A and has primitive bravais lattice properties. As much as 20 wt% of nickel can be intercalated and supported to bleaching clay. Metal supported clay have low load capacity compared with metal intercalated clay. However, particle diameter and surface area are increasing from 90 A to 170 A and 600 m 2 /g to 800 m 2 /g when load capacity is increases. Reactivity of Ni(II) supported bleaching clay is low where percentage of saturated fatty acid increases by 1 % to 2.5 % in hydrogenation reaction of crude palm oil at room temperature and pressure. 2012-01 Undergraduates Project Papers NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/7797/1/MOHD_ALIAS_BIN_AHMAD.PDF Mohd Alias, Ahmad (2012) Synthesis, characterization and catalytic activity of Ni supported on bleaching clay. Faculty of Industrial Sciences & Technology, Universiti Malaysia Pahang. http://iportal.ump.edu.my/lib/item?id=chamo:76298&theme=UMP2
repository_type	Digital Repository
institution_category	Local University
institution	Universiti Malaysia Pahang
building	UMP Institutional Repository
collection	Online Access
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Mohd Alias, Ahmad Synthesis, characterization and catalytic activity of Ni supported on bleaching clay
description	Bleaching clay samples from Hudson WA Sdn Bhd were used to synthesis Ni(II) supported on clay. Metal supported on clay can serve as catalyst for hydrogenation reaction of crude palm oil. Acid analyses were employed using Ion Chromatography and titration technique to determine type and acid content. The nature of the bleaching clay examined by using X-ray Diffraction (XRI)), Thermal Gravimetric Analysis (TGA), Fourier Transform Infrared (FTIR) and BET surface area. Nickel acetate with ethylene glycol as reducing agent was treated with bleaching clay to absorp metal: onto and into the interlayer of the clay. The adsorption of Ni(II) was investigated using BET surface area and x-ray diffraction. IC analysis and acid-base titration showed acid sulphuric as dominant acid at 0.0615 wt %. FTIR spectra and XRD pattern of this clay is identical with jute mineral It has a lattice spacing of 10.67 A and has primitive bravais lattice properties. As much as 20 wt% of nickel can be intercalated and supported to bleaching clay. Metal supported clay have low load capacity compared with metal intercalated clay. However, particle diameter and surface area are increasing from 90 A to 170 A and 600 m 2 /g to 800 m 2 /g when load capacity is increases. Reactivity of Ni(II) supported bleaching clay is low where percentage of saturated fatty acid increases by 1 % to 2.5 % in hydrogenation reaction of crude palm oil at room temperature and pressure.
format	Undergraduates Project Papers
author	Mohd Alias, Ahmad
author_facet	Mohd Alias, Ahmad
author_sort	Mohd Alias, Ahmad
title	Synthesis, characterization and catalytic activity of Ni supported on bleaching clay
title_short	Synthesis, characterization and catalytic activity of Ni supported on bleaching clay
title_full	Synthesis, characterization and catalytic activity of Ni supported on bleaching clay
title_fullStr	Synthesis, characterization and catalytic activity of Ni supported on bleaching clay
title_full_unstemmed	Synthesis, characterization and catalytic activity of Ni supported on bleaching clay
title_sort	synthesis, characterization and catalytic activity of ni supported on bleaching clay
publishDate	2012
url	http://umpir.ump.edu.my/id/eprint/7797/ http://umpir.ump.edu.my/id/eprint/7797/ http://umpir.ump.edu.my/id/eprint/7797/1/MOHD_ALIAS_BIN_AHMAD.PDF
first_indexed	2023-09-18T22:04:48Z
last_indexed	2023-09-18T22:04:48Z
_version_	1777414636072599552

Synthesis, characterization and catalytic activity of Ni supported on bleaching clay

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