Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration

Uniform, well-dispersed, silver nanoparticles (AgNPs) were prepared by a simple chemical reduction method. The particles were synthesized via the reduction of AgNO3 by trisodium citrate and ascorbic acid as a surfactant. The resulting AgNPs were characterized by X-ray diffraction analysis, transmis...

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Main Authors: Suriati, Ghazali, Mariatti, Jaafar, Azizan, Aziz
Format: Article
Language:English
Published: Universiti Malaysia Pahang 2014
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/8239/
http://umpir.ump.edu.my/id/eprint/8239/
http://umpir.ump.edu.my/id/eprint/8239/
http://umpir.ump.edu.my/id/eprint/8239/1/Synthesis_of_Silver_Nanoparticles_By_Chemical_Reduction_Method-_Effect_of_Reducing_Agent_and_Surfactant_Concentration.pdf
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spelling ump-82392018-02-08T03:39:55Z http://umpir.ump.edu.my/id/eprint/8239/ Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration Suriati, Ghazali Mariatti, Jaafar Azizan, Aziz TP Chemical technology Uniform, well-dispersed, silver nanoparticles (AgNPs) were prepared by a simple chemical reduction method. The particles were synthesized via the reduction of AgNO3 by trisodium citrate and ascorbic acid as a surfactant. The resulting AgNPs were characterized by X-ray diffraction analysis, transmission electron microscopy, and scanning electron microscopy. It was found that the size of the AgNPs ranged from 35–80 nm, with an average of 50 nm. In this study, the effects of trisodium citrate and ascorbic acid, which act as reducing agent and surfactant respectively on the morphology of the silver nanoparticles, were investigated. It was found that the increasing concentration of trisodium citrate resulted in decreasing size of silver nanoparticles, while increasing the concentration of ascorbic acid shows the opposite effect. Moreover, the quasi-spherical shape of as-synthesized silver nanoparticles is also more uniform with the increase of trisodium citrate. Meanwhile, a slight change in particle shape from quasi-spherical to polygonal was observed as the concentrations of ascorbic acid were increased. Universiti Malaysia Pahang 2014 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/8239/1/Synthesis_of_Silver_Nanoparticles_By_Chemical_Reduction_Method-_Effect_of_Reducing_Agent_and_Surfactant_Concentration.pdf Suriati, Ghazali and Mariatti, Jaafar and Azizan, Aziz (2014) Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration. International Journal of Automotive and Mechanical Engineering (IJAME), 105. pp. 1920-1927. ISSN 2229-8649 (Print); 2180-1606 (Online) http://dx.doi.org/10.15282/ijame.10.2014.9.0160 DOI: 10.15282/ijame.10.2014.9.0160
repository_type Digital Repository
institution_category Local University
institution Universiti Malaysia Pahang
building UMP Institutional Repository
collection Online Access
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Suriati, Ghazali
Mariatti, Jaafar
Azizan, Aziz
Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration
description Uniform, well-dispersed, silver nanoparticles (AgNPs) were prepared by a simple chemical reduction method. The particles were synthesized via the reduction of AgNO3 by trisodium citrate and ascorbic acid as a surfactant. The resulting AgNPs were characterized by X-ray diffraction analysis, transmission electron microscopy, and scanning electron microscopy. It was found that the size of the AgNPs ranged from 35–80 nm, with an average of 50 nm. In this study, the effects of trisodium citrate and ascorbic acid, which act as reducing agent and surfactant respectively on the morphology of the silver nanoparticles, were investigated. It was found that the increasing concentration of trisodium citrate resulted in decreasing size of silver nanoparticles, while increasing the concentration of ascorbic acid shows the opposite effect. Moreover, the quasi-spherical shape of as-synthesized silver nanoparticles is also more uniform with the increase of trisodium citrate. Meanwhile, a slight change in particle shape from quasi-spherical to polygonal was observed as the concentrations of ascorbic acid were increased.
format Article
author Suriati, Ghazali
Mariatti, Jaafar
Azizan, Aziz
author_facet Suriati, Ghazali
Mariatti, Jaafar
Azizan, Aziz
author_sort Suriati, Ghazali
title Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration
title_short Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration
title_full Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration
title_fullStr Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration
title_full_unstemmed Synthesis of Silver Nanoparticles By Chemical Reduction Method: Effect of Reducing Agent and Surfactant Concentration
title_sort synthesis of silver nanoparticles by chemical reduction method: effect of reducing agent and surfactant concentration
publisher Universiti Malaysia Pahang
publishDate 2014
url http://umpir.ump.edu.my/id/eprint/8239/
http://umpir.ump.edu.my/id/eprint/8239/
http://umpir.ump.edu.my/id/eprint/8239/
http://umpir.ump.edu.my/id/eprint/8239/1/Synthesis_of_Silver_Nanoparticles_By_Chemical_Reduction_Method-_Effect_of_Reducing_Agent_and_Surfactant_Concentration.pdf
first_indexed 2023-09-18T22:05:36Z
last_indexed 2023-09-18T22:05:36Z
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