Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy
Fourier transform infrared (FTIR) spectroscopy, in combination with attenuated total reflectance (ATR) and partial least square (PLS) regression, was used to detect the presence of lard in chocolate formulation. The spectral bands associated with lard, cocoa butter and their blends (ranging from 0%...
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iium-72212012-05-07T07:53:46Z http://irep.iium.edu.my/7221/ Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy Che Man, Yakoob Syahariza, Z. A. Mirghani, Mohamed Elwathig Saeed Jinab, Selamat Bakar, Jamilah T Technology (General) Fourier transform infrared (FTIR) spectroscopy, in combination with attenuated total reflectance (ATR) and partial least square (PLS) regression, was used to detect the presence of lard in chocolate formulation. The spectral bands associated with lard, cocoa butter and their blends (ranging from 0% to 15% of lard in cocoa butter) were recorded, interpreted and identified. A semi-quantitative approach is proposed to measure the percent of lard in blends on the basis of spectral data at the frequency region 4000–650 cm−1, using the equation y = 0.9225x + 0.5539. The coefficient of determination (R2) was 0.9872 with a standard error (SE) of 1.305. In this paper, the potential of FTIR spectroscopy as a rapid analytical tool for the quantitative determination of adulterants especially lard, in chocolate, is demonstrated. Elsevier 2005 Article PeerReviewed application/pdf en http://irep.iium.edu.my/7221/1/Syahariza_%28Lard_in_Chocolate%29.pdf Che Man, Yakoob and Syahariza, Z. A. and Mirghani, Mohamed Elwathig Saeed and Jinab, Selamat and Bakar, Jamilah (2005) Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy. Food Chemistry, 90. pp. 815-819. ISSN 0308-8146 |
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T Technology (General) Che Man, Yakoob Syahariza, Z. A. Mirghani, Mohamed Elwathig Saeed Jinab, Selamat Bakar, Jamilah Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy |
description |
Fourier transform infrared (FTIR) spectroscopy, in combination with attenuated total reflectance (ATR) and partial least square (PLS) regression, was used to detect the presence of lard in chocolate formulation. The spectral bands associated with lard, cocoa butter and their blends (ranging from 0% to 15% of lard in cocoa butter) were recorded, interpreted and identified. A semi-quantitative approach is proposed to measure the percent of lard in blends on the basis of spectral data at the frequency region 4000–650 cm−1, using the equation y = 0.9225x + 0.5539. The coefficient of determination (R2) was 0.9872 with a standard error (SE) of 1.305. In this paper, the potential of FTIR spectroscopy as a rapid analytical tool for the quantitative determination of adulterants especially lard, in chocolate, is demonstrated.
|
format |
Article |
author |
Che Man, Yakoob Syahariza, Z. A. Mirghani, Mohamed Elwathig Saeed Jinab, Selamat Bakar, Jamilah |
author_facet |
Che Man, Yakoob Syahariza, Z. A. Mirghani, Mohamed Elwathig Saeed Jinab, Selamat Bakar, Jamilah |
author_sort |
Che Man, Yakoob |
title |
Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy |
title_short |
Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy |
title_full |
Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy |
title_fullStr |
Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy |
title_full_unstemmed |
Analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy |
title_sort |
analysis of potential lard adulteration in chocolate and chocolate products using fourier transform infrared spectroscopy |
publisher |
Elsevier |
publishDate |
2005 |
url |
http://irep.iium.edu.my/7221/ http://irep.iium.edu.my/7221/1/Syahariza_%28Lard_in_Chocolate%29.pdf |
first_indexed |
2023-09-18T20:16:31Z |
last_indexed |
2023-09-18T20:16:31Z |
_version_ |
1777407823597010944 |